“…l-(2-Hydroxyethoxy)norbornane (3, R = OCH2CH2OH) was obtained as a clear oil: rmax (CCI4) 3431, 2957, 2925, 2872, 1452, 1319, 1262, 1179, 1141, 1071, and 891 cm"1; NMR (CDC13) r 6.31 (m, 4, CH2CH2), 7.5 (s, 1, OH) and 7.87 (br s, 1, CH-4); m/e 156.1148 (caled for C9H1602, 156.1150), 127 (39), 113 (34), 95 (25), and 83 (100). 1 -m-and -p-Tolylnorbornane (3, R = m-and p-CH3C6H4) were isolated as a mixture: ¡Wx (neat) 3055, 3025, 2950, 2922, 2873, 1603, 1508, 1486, 1450, 1329, 1300, 802, 773, and 695 cm"1; >H NMR (CDC13) t 2.73 (m, 5, aromatic H) and 7.64 (s, 3, Ar-CH3); m/e 186.1405 (caled for CI4HI8, 186.1408), 186 (45), and 147 (100).…”