The synthesis of 2,6,7‐trioxa‐1,4‐diphosphabicyclo[2.2.2]octane revisited: the synthesis of 2,6,7‐triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane and the synthesis of 1λ5‐phosphiranol

Kisanga, Philip; Verkade, John G.

doi:10.1002/hc.8

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The synthesis of 2,6,7‐trioxa‐1,4‐diphosphabicyclo[2.2.2]octane revisited: the synthesis of 2,6,7‐triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane and the synthesis of 1λ⁵‐phosphiranol

Abstract: ABSTRACT:We report herein a reliable synthesis of P(OCH 2 ) 3 P in a study aimed at understanding the factors that control its formation. We also report the serendipitous synthesis of the novel phosphiranol (CH 2 ) 2 PO 2 H and the synthesis of P(PhNCH 2 ) 3 P in good yield.

Cited by 13 publications

References 8 publications

ChemInform Abstract: The Synthesis of 2,6,7‐Trioxa‐1,4‐diphosphabicyclo[2.2.2]octane (III) Revisited: The Synthesis of 2,6,7‐Triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane (VI) and the Synthesis of 1λ⁵‐Phosphiranol (IV).

ChemInform Abstract: The Synthesis of 2,6,7‐Trioxa‐1,4‐diphosphabicyclo[2.2.2]octane (III) Revisited: The Synthesis of 2,6,7‐Triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane (VI) and the Synthesis of 1λ⁵‐Phosphiranol (IV).

Bridged Dinuclear Tripodal Tris(amido)phosphane Complexes of Titanium and Zirconium as Diligating Building Blocks for Organometallic Polymers

109 Chemical Shifts and Coupling Constants for C3H9O3P

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The synthesis of 2,6,7‐trioxa‐1,4‐diphosphabicyclo[2.2.2]octane revisited: the synthesis of 2,6,7‐triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane and the synthesis of 1λ5‐phosphiranol

Abstract: ABSTRACT:We report herein a reliable synthesis of P(OCH 2 ) 3 P in a study aimed at understanding the factors that control its formation. We also report the serendipitous synthesis of the novel phosphiranol (CH 2 ) 2 PO 2 H and the synthesis of P(PhNCH 2 ) 3 P in good yield.

Cited by 13 publications

References 8 publications

ChemInform Abstract: The Synthesis of 2,6,7‐Trioxa‐1,4‐diphosphabicyclo[2.2.2]octane (III) Revisited: The Synthesis of 2,6,7‐Triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane (VI) and the Synthesis of 1λ5‐Phosphiranol (IV).

ChemInform Abstract: The Synthesis of 2,6,7‐Trioxa‐1,4‐diphosphabicyclo[2.2.2]octane (III) Revisited: The Synthesis of 2,6,7‐Triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane (VI) and the Synthesis of 1λ5‐Phosphiranol (IV).

Bridged Dinuclear Tripodal Tris(amido)phosphane Complexes of Titanium and Zirconium as Diligating Building Blocks for Organometallic Polymers

109 Chemical Shifts and Coupling Constants for C3H9O3P

Contact Info

Product

Resources

About

The synthesis of 2,6,7‐trioxa‐1,4‐diphosphabicyclo[2.2.2]octane revisited: the synthesis of 2,6,7‐triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane and the synthesis of 1λ⁵‐phosphiranol

ChemInform Abstract: The Synthesis of 2,6,7‐Trioxa‐1,4‐diphosphabicyclo[2.2.2]octane (III) Revisited: The Synthesis of 2,6,7‐Triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane (VI) and the Synthesis of 1λ⁵‐Phosphiranol (IV).

ChemInform Abstract: The Synthesis of 2,6,7‐Trioxa‐1,4‐diphosphabicyclo[2.2.2]octane (III) Revisited: The Synthesis of 2,6,7‐Triphenyl‐2N,6N,7N‐triaza‐1,4‐diphosphabicyclo[2.2.2]octane (VI) and the Synthesis of 1λ⁵‐Phosphiranol (IV).