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“…The crystalline compound of 5 sublimed quickly on exposure to the air and gave red color with tetranitromethane in CCU. Pyran 5 shows their absorptions at 1715, 1678, and 812 cm-1; nmr 9.03 (d, J = 4 Hz, 3 H), 8.96 (s, 6 H), 8.32 (d, 1 Hz, 3 H), 5.82 (q, J = 1 Hz, 1 H); plain positive ORD curve ( µ) 32 (550), 41 (500), 50 (450), 70 (400), 95 (350) and 160 (300) in ethanol and 70 (550), 95 (500), 119 (450), 155 (400), 234 (350) and 415 (300) in isooctane.…”
mentioning
confidence: 99%
“…The crystalline compound of 5 sublimed quickly on exposure to the air and gave red color with tetranitromethane in CCU. Pyran 5 shows their absorptions at 1715, 1678, and 812 cm-1; nmr 9.03 (d, J = 4 Hz, 3 H), 8.96 (s, 6 H), 8.32 (d, 1 Hz, 3 H), 5.82 (q, J = 1 Hz, 1 H); plain positive ORD curve ( µ) 32 (550), 41 (500), 50 (450), 70 (400), 95 (350) and 160 (300) in ethanol and 70 (550), 95 (500), 119 (450), 155 (400), 234 (350) and 415 (300) in isooctane.…”
mentioning
confidence: 99%
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