The structure of 6-tert-butyl-4,5-dichloro-3-ethyl-4,5-dihydro-2,1-benzoisoxazole

3-[Chloro(phenyl)methyl]-6-methyl-1,2-benzoxazole

“…1. The bond length and angles are in agreement with those found for closely related structures, for example, 6-tert-butyl-4,5-dichloro-3ethyl-4,5-dihydro-2,1-benzoisoxazole (II) [Atovmyan & Aliev, 1994] [Korlyukov et al, 2003], and N-Phenyl-4-(8-phenyl-4,5-dihydro-1,2-benzoxazolo-[4,5-d]thiazol-2-yl)-piperidine-1carboxamide (IV) [Hu et al, 2009] (Atovmyan & Aliev, 1994). The dihedral angle between the mean plane of the 1,2benzoxazole [max.…”

“…For the synthesis of the title compound, see: Veerareddy et al (2011). For related structures, see: Atovmyan & Aliev (1994); Hu et al (2009); Korlyukov et al (2003). Data collection: APEX2 (Bruker, 2004); cell refinement: APEX2 and SAINT (Bruker, 2004); data reduction: SAINT and XPREP (Bruker, 2004); program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: ORTEP-3 (Farrugia, 1997) and Mercury (Macrae et al, 2008); software used to prepare material for publication: PLATON (Spek, 2009).…”