Journal of Chromatography A volume 1218, issue 51, P9149-9154 2011 DOI: 10.1016/j.chroma.2011.10.085 View full text
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Jing Jin, Yun Li, Zhiping Zhang, Fan Su, Peipei Qi, Xianbo Lu, Jiping Chen

Abstract: a b s t r a c tA new method for the selective cleanup of complex matrices and simultaneous separation of benzo [a]pyrene (BaP) was developed in this study. This method was based on solid-phase extraction (SPE) using magnesium oxide microspheres as sorbents, and it eliminated interferences from various impurities, such as lipids, sulphur, pigments, halobenzenes, polychlorodibenzo-p-dioxins and polychlorodibenzofurans. Several parameters, including the volume of rinsing and eluting solvents, the type of loading…

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