The prostaglandins Vol. 1, edited by P. W. Ramwell. Pp xvii + 400. Plenum Publishing Corporation, New York. 1973. $34.00

Horton, Emily

doi:10.1016/0160-9327(74)90022-2

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“…This transformation is, in fact, routinely used during multistep syntheses of natural and specialty products, in both laboratory and industrial processes. 1 Acetyl chloride 2 and acetic anhydride 3 are usually employed as acetylating agents in the presence of tributylphosphine 4 or pyridine derivatives. 5 Various catalysts developed for acylation include DMAP, 6 CoCl 2 , 22 and alumina.…”

Section: Introductionmentioning

confidence: 99%

Iodine Supported on 3‐Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent‐free Conditions

Mahdavi¹,

Ghaemy

Zeraatpisheh

2009

Chin. J. Chem.

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Section: Introductionmentioning

confidence: 99%

Iodine Supported on 3‐Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent‐free Conditions

Mahdavi¹,

Ghaemy

Zeraatpisheh

2009

Chin. J. Chem.

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“…The acetylation of the hydroxy function of alcohols is an important and frequently used transformation in organic synthesis . Acetic anhydride and acetyl chloride are usually used as the acylating agents. To increase the rate of acylation, the reaction is carried out in the presence of a protic or Lewis acid catalyst .…”

Section: Introductionmentioning

confidence: 99%

An Efficient Acylation of Tertiary Alcohols with Isopropenyl Acetate Mediated by an Oxime Ester and Cp*₂Sm(thf)₂

Tashiro

Kawasaki²,

Sakaguchi³

et al. 1997

J. Org. Chem.

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An efficient method for the acylation of tertiary alcohols with isopropenyl acetate (1) by the use of an oxime and Cp(2)Sm(thf)(2) as catalyst was developed. Thus, various types of tertiary alcohols could be acylated with 1 in the presence of a catalytic amount of cyclohexanone oxime acetate (2) and Cp(2)Sm(thf)(2) under mild conditions to form the corresponding acetates in excellent yields. Acid-sensitive terpene alcohols such as linalool were successfully acetylated by the present method to give acetyl linalool in quantitative yield. This method enables an alternative acylation of tertiary alcohols under acid-free conditions.

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The prostaglandins Vol. 1, edited by P. W. Ramwell. Pp xvii + 400. Plenum Publishing Corporation, New York. 1973. $34.00

Cited by 2 publications

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Iodine Supported on 3‐Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent‐free Conditions

Iodine Supported on 3‐Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent‐free Conditions

An Efficient Acylation of Tertiary Alcohols with Isopropenyl Acetate Mediated by an Oxime Ester and Cp*₂Sm(thf)₂

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The prostaglandins Vol. 1, edited by P. W. Ramwell. Pp xvii + 400. Plenum Publishing Corporation, New York. 1973. $34.00

Cited by 2 publications

References 0 publications

Iodine Supported on 3‐Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent‐free Conditions

Iodine Supported on 3‐Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent‐free Conditions

An Efficient Acylation of Tertiary Alcohols with Isopropenyl Acetate Mediated by an Oxime Ester and Cp*2Sm(thf)2

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An Efficient Acylation of Tertiary Alcohols with Isopropenyl Acetate Mediated by an Oxime Ester and Cp*₂Sm(thf)₂