1964
DOI: 10.1021/jo01029a081
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The Preparation of Cyclic Siliconmethylene Compounds

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Cited by 113 publications
(36 citation statements)
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“…[24] The yield of this procedure is limited due to low selectivity and consequent occurrence of product mixtures. The second synthetic strategy, first established by Kriner, [25] is the elegant cyclization of trialkoxy(chloromethyl)silanes with magnesium.…”
Section: Resultsmentioning
confidence: 99%
“…[24] The yield of this procedure is limited due to low selectivity and consequent occurrence of product mixtures. The second synthetic strategy, first established by Kriner, [25] is the elegant cyclization of trialkoxy(chloromethyl)silanes with magnesium.…”
Section: Resultsmentioning
confidence: 99%
“…4. Curve (a) showed typical absorption peaks of PCS [9]. A broad peak appeared near 3434 cm À 1 and a tiny peak at 1630 cm À 1 (indicated by arrows) corresponded to vibrations of the absorbed water molecules.…”
Section: Resultsmentioning
confidence: 99%
“…TMDSCB was prepared as reported 10) . Butyllithium hexane solution was purchased from Wako Pure Chemical Industry, tert-butyllithium pentane solution was purchased from Kanto Chemical Industry, (trimethylsilylmethyl)lithium pentane solution was obtained from Aldrich, and used as received.…”
Section: Methodsmentioning
confidence: 99%