The preparation of "2-bromo-naphthalene"

Wolfe, Winthrop C; Doukas, Harry M.

doi:10.1021/ed028p472

J. Chem. Educ.

1951

DOI: 10.1021/ed028p472

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The preparation of "2-bromo-naphthalene"

Winthrop C Wolfe¹,

Harry M. Doukas²

Abstract: Presents a procedure for the preparation of "2-bromo-naphthalene" in large or small amounts.

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“…3 Geller Microanalytieal Laboratories, Bardonia, N. Y. 4 The gas chromatography data were obtained on a Beckman Model 2-A gas chromatography unit. The column was 6 ft. X 7, in.…”

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confidence: 99%

An improved synthesis of 2-bromonaphthalene

Vingiello¹,

Delia²,

Polss³

et al. 1963

J. Chem. Educ.

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“…3 Geller Microanalytieal Laboratories, Bardonia, N. Y. 4 The gas chromatography data were obtained on a Beckman Model 2-A gas chromatography unit. The column was 6 ft. X 7, in.…”

mentioning

confidence: 99%

An improved synthesis of 2-bromonaphthalene

Vingiello¹,

Delia²,

Polss³

et al. 1963

J. Chem. Educ.

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Preparation of 5-Bromo-2-naphthol: The Use of a Sulfonic Acid as a Protecting and Activating Group

Everett

Hamilton

Abelt

2009

Molbank

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Abstract:The preparation of 5-bromo-2-naphthol (4) in three steps from 5-amino-2-naphthol (1) is described. A sulfonic acid group is introduced at the 1-position as an activating and protecting group for the Sandmeyer reaction. The sulfonate group allows for the use of only water and sulfuric acid as solvents. The sulfonic acid is introduced with three equivalents of sulfuric acid, and it is removed in 20% aq. sulfuric acid.

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The preparation of "2-bromo-naphthalene"

Abstract: Presents a procedure for the preparation of "2-bromo-naphthalene" in large or small amounts.

Cited by 2 publications

References 0 publications

An improved synthesis of 2-bromonaphthalene

An improved synthesis of 2-bromonaphthalene

Preparation of 5-Bromo-2-naphthol: The Use of a Sulfonic Acid as a Protecting and Activating Group

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