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2022

DOI: 10.1016/j.heliyon.2022.e09202

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The heterospin cobalt complexes: peculiarities of high-resolution NMR spectra

¹

,

Igor А. Ushakov

²

,

Evgenia A. Funtikova

³

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H Nmr Spectroscopy1

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Cited by 3 publications

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“…In general, a broadening and shift to high ppm values of all the peaks were observed, consistent with the presence of a paramagnetic complex in the two Co containing systems compared to the neat EG : ChCl (4.5 : 1). [69][70][71] All the chemical shift values of protons in the neat solvent system and the two Co containing systems are given in Table 1.…”

Section: H Nmr Spectroscopymentioning

confidence: 99%

A case study using spectroscopy and computational modelling for Co speciation in a deep eutectic solvent

Perera,

Dobhal,

Pringle

et al. 2024

Phys. Chem. Chem. Phys.

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Co(ii) speciation is reported for two ethylene glycol : choline chloride (4.5 : 1) systems depending on the cobalt source using several spectroscopic techniques (e.g. UV-Vis, NMR, EPR, FTIR) in combination with molecular dynamics simulations.

“…In general, a broadening and shift to high ppm values of all the peaks were observed, consistent with the presence of a paramagnetic complex in the two Co containing systems compared to the neat EG : ChCl (4.5 : 1). [69][70][71] All the chemical shift values of protons in the neat solvent system and the two Co containing systems are given in Table 1.…”

Section: H Nmr Spectroscopymentioning

confidence: 99%

A case study using spectroscopy and computational modelling for Co speciation in a deep eutectic solvent

Perera,

Dobhal,

Pringle

et al. 2024

Phys. Chem. Chem. Phys.

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Co(ii) speciation is reported for two ethylene glycol : choline chloride (4.5 : 1) systems depending on the cobalt source using several spectroscopic techniques (e.g. UV-Vis, NMR, EPR, FTIR) in combination with molecular dynamics simulations.

Theoretical and practical aspects of indirect spin–spin couplings

Jaźwiński

2023

Nuclear Magnetic Resonance

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This survey gathered works on various aspects of indirect spin–spin coupling constants: new calculation approaches, comparison of calculated and experimental values, indirect spin–spin coupling constants involving heavy nuclei, through space coupling constants and measurements in the gas phase. This review covers the period from May 2022 to April 2023.

Synthesis of a tube-like tetra-bipyridyl, tetra-ethylacetato-calix[4]arene in 1,3-alternate conformation and the unexpected crystal structure of its [bpy(CoCl₂)]₃-[bpy(CoCl₂)(H₂O)] complex

Mourer,

Bouizi,

Leclerc

et al. 2024

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Treating the conic tetra-para-ethylacetato-calix[4]arene 1 with 2.2 equivalents of K2CO3 and 4 equivalents of 6-bromomethyl-6’-methyl-2,2’-bipyridine afford the expected fully substituted podand, mainly in its 1,3-alternate conformation 2. This tube-like bipyridyl...

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