We present observations of NOAA solar Active Region 7999 when it was near the west solar limb on 1996 December 2 and 3, using data from the Coronal Diagnostic Spectrometer (CDS) experiment on the SOHO satellite. Ratios of intensities of 2 MK material (as observed in CDS Fe XVI images) to 1 MK material (from CDS Mg IX images) indicate that there is a drop in the ratio of the hotter to the cooler material with height in the region, up to an altitude of about 105 km. At low altitudes the relative amount of 2 MK emission measure to 1 MK emission measure ranges from 8 to 10, while the ratio is minimum near 105 km, ranging from 1.3 to 3.5. The decrease with height of the CDS ratio qualitatively resembles the decrease in S XV election temperature with height (measurable up to B85,000 km) in the same active region obtained from the Bragg crystal spectrometer instrument on Y ohkoh. The CDS images indicate that the highest S XV temperatures and largest CDS ratios correspond to regions of microÑares, and somewhat lower S XV temperatures and CDS ratios correspond to di †use regions. Above 105 km, the trend of the CDS ratios changes, either increasing or remaining approximately constant with height. At these altitudes the CDS images show faint, large-scale di †use structures.