The evolution of long-period stacking ordered phase and its effect on dynamic recrystallization in Mg-Gd-Y-Zn-Zr alloy processed by repetitive upsetting-extrusion

Meng, Yingze; Yu, Jianmin; Li, Kai; Yu, Huisheng; Zhang, Fan; Wu, Yuna; Zhang, Zhimin; Luo, Nina; Wang, Honghai

doi:10.1016/j.jallcom.2020.154454

Cited by 60 publications

(13 citation statements)

References 39 publications

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“…At 3 passes, the edge of the block-shaped phase is not smooth and breaks. Some of the blockshaped phases are broken into dense small masses due to the stress concentration (as shown by the black arrow in the Figure 4c), similar to the phenomenon we observed in repetitive upsettingextrusion before [34]. The large lamellar phase is reduced, and the kink phenomenon is weakened, indicating that the strain of the alloy is more uniform under this condition.…”

Section: Microstructure Evolution Of the Mdfed Alloyssupporting

confidence: 78%

“…It can be observed from Figure 10 that the block-shaped phases are distributed at the grain boundaries of the dynamic recrystallization region (blue arrow in Figure 10 ), and they are almost completely surrounded by dynamic recrystallization. Studies have shown that stress concentration is more likely to occur around the block-shaped phase, which is conducive to the plugging of dislocations and becomes the preferential nucleation site for new grains, promoting the occurrence of dynamic recrystallization [ 34 ]. At 1 pass ( Figure 10 a), the phenomenon is more obvious; DRX tends to occur near the block-shaped phase, but only a small amount occurs inside the large lamellar phase area, indicating that the block-shaped phase plays a greater role in promoting the dynamic recrystallization process than the lamellar phase with kinks.…”

Section: Discussionmentioning

confidence: 99%

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The Role of Long Period Stacking Ordered Phase in Dynamic Recrystallization of a Mg–Gd–Y–Zn–Zr Alloy during Multi-Directional Forging Process

Liu

Meng

et al. 2020

Materials

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The Mg–Gd–Y–Zn–Zr alloy containing a long period stacking ordered (LPSO) phase was subjected to multi-pass deformation by means of a multi-directional forging process, and the microstructure evolution and the influence of the LPSO phase on its dynamic recrystallization (DRX) were studied. The results showed that multi-directional forging can effectively refine the grain with the DRX fraction increased, and DRXed grains lead to the decrease of the texture intensity, which can significantly improve the mechanical properties of the alloy. The different morphologies of the LPSO phase have different degrees of promotion relative to DRX behavior. The lamellar LPSO phase with kinks promoted dislocation plugging, where there could be a potential nucleation site for DRX grains. The fragmented lamellar LPSO phase promoted the DRX process through the particle-stimulated nucleation mechanism, and the block-shaped phase was more prone to stress concentration, which promoted DRX. These effects resulted in continuous grain refinement and a more uniform microstructure.

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Section: Microstructure Evolution Of the Mdfed Alloyssupporting

confidence: 78%

Section: Discussionmentioning

confidence: 99%

The Role of Long Period Stacking Ordered Phase in Dynamic Recrystallization of a Mg–Gd–Y–Zn–Zr Alloy during Multi-Directional Forging Process

Liu

Meng

et al. 2020

Materials

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“…Metals 2020, 10, x FOR PEER REVIEW 4 of 11 particle phases precipitated at the DRX grain boundaries, which indicated that the alloy had undergone dynamic precipitation during the RUE deformation process. The slippage of the particles relative to the grain boundaries plays a pinning role, inhibiting the growth of dynamic recrystallized grains during thermal deformation and during heating between passes [24]. With the increasing number of the RUE passes, the size of the remaining coarse grains gradually decreases, and the number of DRX grains continues to increase, surrounding the coarse grains.…”

Section: Microstructure Evolution Of the Rue Alloysmentioning

confidence: 99%

Effect of Decreasing Temperature Reciprocating Upsetting-Extrusion on Microstructure and Mechanical Properties of Mg-Gd-Y-Zr Alloy

et al. 2020

Metals

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The decreasing temperature reciprocating upsetting-extrusion (RUE) deformation experiment was carried out on Mg-Gd-Y-Zr alloy to study RUE deformation on the influence of microstructure of the alloy. This work showed that with the gradual increase of RUE deformation passes, the continuous dynamic recrystallization (CDRX) process and the discontinuous dynamic recrystallization (DDRX) process occurred at the same time, and the grain refinement effect was obvious. Particulate precipitation induced the generation of DRX through particle-stimulated nucleation (PSN). In addition, after one pass of RUE deformation, the alloy produced a strong basal texture. As the RUE experiment proceeded, the basal texture intensity decreased. The weakening of the texture was due to the combined effect of DRX and alternating loading forces in the axial and radial directions. After four RUE passes, the mechanical properties of the alloy had been significantly improved, which was the result of the combined effect of dislocation strengthening, fine grain strengthening, and second phase strengthening.

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“…The LPSO phase in Mg-RE alloy has abundant structural morphologies and excellent properties. It has rapidly become the most promising structural material in the field of metal materials [ 21 , 22 , 23 ], thereby attracting great attention and leading to the upsurge of research on the atomic arrangement, formation mechanism, and mechanical properties of LPSO phase.…”

Section: Introductionmentioning

confidence: 99%

The Formation of 14H-LPSO in Mg–9Gd–2Y–2Zn–0.5Zr Alloy during Heat Treatment

Liu

Yang

et al. 2021

Materials

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There is a new long-period stacking ordered structure in Mg–RE–Zn magnesium alloys, namely the LPSO phase, which can effectively improve the yield strength, elongation, and corrosion resistance of Mg alloys. According to different types of Mg–RE–Zn alloy systems, two transformation modes are involved in the heat treatment transformation process. The first is the alloy without LPSO phase in the as-cast alloy, and the MgxRE phase changes to 14H-LPSO phase. The second is the alloy containing LPSO phase in the as-cast state, and the 14H-LPSO phase is obtained by the transformations of 6H, 18R, and 24R. The effects of different solution parameters on the second phase of Mg–9Gd–2Y–2Zn–0.5Zr alloy were studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray diffraction (XRD). The precipitation mechanism of 14H-LPSO phase during solution treatment was further clarified. At a solution time of 13 h, the grain size increased rapidly initially and then decreased slightly with increasing solution temperature. The analysis of the volume fraction of the second phase and lattice constant showed that Gd and Y elements in the alloy precipitated from the matrix and formed 14H-LPSO phase after solution treatment at 490 °C for 13 h. At this time, the hardness of the alloy reached the maximum of 74.6 HV. After solution treatment at 500 °C for 13 h, the solid solution degree of the alloy increases, and the grain size and hardness of the alloy remain basically unchanged.

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The evolution of long-period stacking ordered phase and its effect on dynamic recrystallization in Mg-Gd-Y-Zn-Zr alloy processed by repetitive upsetting-extrusion

Cited by 60 publications

References 39 publications

The Role of Long Period Stacking Ordered Phase in Dynamic Recrystallization of a Mg–Gd–Y–Zn–Zr Alloy during Multi-Directional Forging Process

The Role of Long Period Stacking Ordered Phase in Dynamic Recrystallization of a Mg–Gd–Y–Zn–Zr Alloy during Multi-Directional Forging Process

Effect of Decreasing Temperature Reciprocating Upsetting-Extrusion on Microstructure and Mechanical Properties of Mg-Gd-Y-Zr Alloy

The Formation of 14H-LPSO in Mg–9Gd–2Y–2Zn–0.5Zr Alloy during Heat Treatment

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