“…From these various studies it is obvious that sugars significantly affect the gelation and retrogradation of starch depending on the types of sugar and starch. Although many experiments on the gelation and retrogradation of starch-sugar composites have been performed by using differential scanning calorimetry (Ahmad & Williams, 1999;Billiadris & Prokopowich, 1994;Chang & Liu, 1991;Lii, Lai, & Liu, 1998;Wang & Jane, 1994), nuclear magnetic resonance (Boltan & Desbois, 1995;Farhat, Blanshard, Descamps, & Mitchell, 2000), and X-ray diffraction (Cairns et al, 1991;Farhat et al, 2000;Hoover & Senanayake, 1996;I'Anson et al, 1990), dynamic rheometry can provide a useful probe to monitor the kinetics of structure development of physical cross-links either in the form of simple chain entanglements or crystallite formation by amylopectin (Prokopowich & Biliaderis, 1995). It also allows continuous measurement of the dynamic moduli without breaking structural elements formed in the sample on cooling and aging.…”