Abstract:− Zirconium hydroxide was synthesized by varying the aging time of the zirconyl chloride octahydrate at 100 o C in aqueous solution and the resulting hydroxides were calcined at 700 o C for 6 h to obtain the crystalline ZrO 2 . The materials used in this study were characterized by differential thermal analysis (DTA), X-ray diffraction (XRD), N 2 -sorption, transmission electron microscopy (TEM), NH 3 temperature-programmed desorption (NH 3 -TPD), CO 2 -TPD and iso-propanol TPD analyses to correlate with catal… Show more
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