Abstract:The curing kinetics can influence the final macroscopic properties, particularly the three-point bending of the fiber-reinforced composite materials. In this research, the curing kinetics of commercially available glass fiber/epoxy resin prepregs were studied by non-isothermal differential scanning calorimetry (DSC). The curing kinetic parameters were obtained by fitting and the apparent activation energy Ea of the prepreg, the pre-exponent factor, and the reaction order value obtained. A phenomenological nth-… Show more
“…The second heating scan reveals that the GF laminate samples are entirely cured. Lvtao Zhu et al [ 19 ] presented similar results in a recent work.…”
Section: Resultssupporting
confidence: 67%
“…The second heating scan reveals that the GF laminate samples are entirely cured. Lvtao Zhu et al [19] presented similar results in a recent work. The previous observations show that time is not relevant for the curing process, the reason sample 4 can be discarded.…”
Sandwich composites are widely used in the manufacture of aircraft cabin interior panels for commercial aircraft, mainly due to the light weight of the composites and their high strength-to-weight ratio. Panels are used for floors, ceilings, kitchen walls, cabinets, seats, and cabin dividers. The honeycomb core of the panels is a very light structure that provides high rigidity, which is considerably increased with fiberglass face sheets. The panels are manufactured using the compression molding process, where the honeycomb core is crushed up to the desired thickness. The crushed core breaks fiberglass face sheets and causes other damage, so the panel must be reworked. Some damage is associated with excessive build-up of resin in localized areas, incomplete curing of the pre-impregnated fiberglass during the manufacturing process, and excessive temperature or residence time during the compression molding. This work evaluates the feasibility of using rigid polyurethane foams as a substitute for the honeycomb core. The thermal and viscoelastic behavior of the cured prepreg fiberglass under different manufacturing conditions is studied. The first part of this work presents the influence of the manufacturing parameters and the feasibility of using rigid foams in manufacturing flat panels oriented to non-structural applications. The conclusion of the article describes the focus of future research.
“…The second heating scan reveals that the GF laminate samples are entirely cured. Lvtao Zhu et al [ 19 ] presented similar results in a recent work.…”
Section: Resultssupporting
confidence: 67%
“…The second heating scan reveals that the GF laminate samples are entirely cured. Lvtao Zhu et al [19] presented similar results in a recent work. The previous observations show that time is not relevant for the curing process, the reason sample 4 can be discarded.…”
Sandwich composites are widely used in the manufacture of aircraft cabin interior panels for commercial aircraft, mainly due to the light weight of the composites and their high strength-to-weight ratio. Panels are used for floors, ceilings, kitchen walls, cabinets, seats, and cabin dividers. The honeycomb core of the panels is a very light structure that provides high rigidity, which is considerably increased with fiberglass face sheets. The panels are manufactured using the compression molding process, where the honeycomb core is crushed up to the desired thickness. The crushed core breaks fiberglass face sheets and causes other damage, so the panel must be reworked. Some damage is associated with excessive build-up of resin in localized areas, incomplete curing of the pre-impregnated fiberglass during the manufacturing process, and excessive temperature or residence time during the compression molding. This work evaluates the feasibility of using rigid polyurethane foams as a substitute for the honeycomb core. The thermal and viscoelastic behavior of the cured prepreg fiberglass under different manufacturing conditions is studied. The first part of this work presents the influence of the manufacturing parameters and the feasibility of using rigid foams in manufacturing flat panels oriented to non-structural applications. The conclusion of the article describes the focus of future research.
“…The non-model fitting method is based on the assumption of equal conversion, that is, when the curing degree is the same, the reaction rate of the system is only related to temperature [ 43 ]. It avoids the premise that the model fitting method needs to assume the reaction mechanism function in advance and has a good fitting effect on complex reactions [ 44 ].…”
Anhydride-cured bisphenol-A epoxy resin is widely used in the support, insulation and sealing key components of electrical and electronic equipment due to their excellent comprehensive performance. However, overheating and breakdown faults of epoxy resin-based insulation occur frequently under conditions of large current carrying and multiple voltage waveforms, which seriously threaten the safe and stable operation of the system. The curing regime, including mixture ratio and combination of curing time and temperature, is an important factor to determine the microstructure of epoxy resin, and also directly affects its macro performances. In this paper, the evolution of curing kinetic models of anhydride-cured epoxy resin was introduced to determine the primary curing regime. The influences of curing regime on the insulation performance were reviewed considering various mixture ratios and combinations of curing time and temperature. The curing regime-dependent microstructure was discussed and attributed to the mechanisms of insulation performance.
“…The study of resin curing kinetic parameters has theoretical significance for resin application (Chen et al, 2008;Moreau, 2021;Zhu et al, 2021;Cruz-Cruz et al, 2022). The curing kinetic equations involve a variety of parameters that have important implications for understanding the curing reaction, such as the apparent activation energy (E α ) and the reaction energy level (n).…”
One of the most significant defects, porosity, has been proven to affect the properties of composites. It is critical to reduce the porosity of composite material and the curing cost while maintaining high laminate quality for vacuum bag-only prepreg. In this paper, a rapidly cured epoxy resin system was developed, and an alkali-free glass fiber fabric prepreg suitable for vacuum bag molding was prepared by the asymmetric impregnation method. The optimal curing process for the prepreg was determined by resin curing kinetics, dielectric viscosity, initial curing temperature, and curing time of the prepreg on the laminate quality. The optimal curing profile of the prepreg was obtained. In addition, the effect of room temperature exposure time on the properties of the prepreg was also evaluated. These laminates produced by vacuum bag molding had outstanding internal quality and mechanical properties via the changes in the asymmetric impregnation process and the curing procedure.
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