The Crystal Structure of Bis(diethylammonium) Hexachloridoplumbate(IV) Derived From Powder Diffraction Data and its Relation to Structurally Related Hexachloridometallate Salts
C14H18N8O8SnCl6, monoclinic, P21/n (no. 14), a = 8.1810(2) Å, b = 12.6195(3) Å, c = 11.3811(2) Å, β = 90.258(2)°, Z = 2, V = 1174.97(5) Å3, R
gt(F) = 0.0266, wR
ref = 0.0620, T = 290 K.
C10H16N2SnCl6, monoclinic, I2 (no. 5), a = 14.0477(4) Å, b = 8.9140(2) Å, c = 27.6199(6) Å, β = 93.060(2)°, Z = 8, V = 3453.67(15) Å3, R
gt
(F) = 0.0395, wR
ref
= 0.0858, T = 290 K.
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