The crystal structure of 5-(2-(4-fluorophenyl)hydrazono)-4-methyl-2-((3-(5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazol-4-yl)-1-phenyl-1H-pyrazol-4-yl)methylene) hydrazono)-2,5-dihydrothiazole dimethylformamide monosolvate, C₃₀H₂₅FN₁₀S⋅C₃H₇NO

Abstract

<jats:title>Abstract</jats:title><jats:p>C<jats:sub>30</jats:sub>H<jats:sub>25</jats:sub>FN<jats:sub>10</jats:sub>S⋅C<jats:sub>3</jats:sub>H<jats:sub>7</jats:sub>NO, triclinic, <jats:italic>P</jats:italic>1̄ (no. 2), <jats:italic>a</jats:italic> = 10.9189(6) Å, <jats:italic>b</jats:italic> = 12.3898(7) Å, <jats:italic>c</jats:italic> = 13.9206(7) Å, <jats:italic>α</jats:italic> = 199.412(4)°, <jats:italic>β</jats:italic> = 110.024(5)°, <jats:italic>γ</jats:italic> = 105.904(5)°, <jats:italic>V</jats:italic> = 1631.17(17) Å<jats:sup>3</jats:sup>, <jats:italic>Z</jats:italic> = 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub>(<jats:italic>F</jats:italic>) = 0.0536, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub>(<jats:italic>F</jats:italic><jats:sup>2</jats:sup>) = 0.1471, <jats:italic>T</jats:italic> = 296 K.</jats:p>

Synthesis and Structure Determination of 2-Cyano-3-(1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl)acrylamide

“…In this paper, we report the synthesis and characterization of 2-cyano-3-(1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl)acrylamide (3). The structures of several related compounds that contain the pyrazole and thiophene ring systems have been reported [23][24][25][26][27].…”