The Comparison of Derivatization Methods for the Determination of Ethylene Glycol in Lubricant Oil Sample by GC/MS

Lee, Joon-Bae; Kwon, O-Seong; You, Jing; Shon, Shungkun; Paeng, Ki‐Jung; Sung, Tae-Myung

doi:10.5012/bkcs.2012.33.12.4243

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2016

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Cited by 2 publications

(2 citation statements)

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“…We adopted CH‐one among the C4–C7 cycloalkanone reagents, following our previous report . EG reacts with CH‐one to form a spiro‐dioxolane, 1,4‐dioxaspiro [4.5]decane (CAS no.…”

Section: Spme Fibers Usedmentioning

confidence: 99%

On‐fiber Derivatization for Determination of Ethylene Glycol Concentration in Lubricant oil By SPME‐GC/MS

Lee

Shon

Kwon

et al. 2016

Bulletin Korean Chem Soc

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“…We adopted CH‐one among the C4–C7 cycloalkanone reagents, following our previous report . EG reacts with CH‐one to form a spiro‐dioxolane, 1,4‐dioxaspiro [4.5]decane (CAS no.…”

Section: Spme Fibers Usedmentioning

confidence: 99%

On‐fiber Derivatization for Determination of Ethylene Glycol Concentration in Lubricant oil By SPME‐GC/MS

Lee

Shon

Kwon

et al. 2016

Bulletin Korean Chem Soc

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“…Glycols are converted into benzyl ethers [2,3] and determined by using HPLC. In the gas-chromatographic (GC) determination, glycols are converted into methyl [4] and trimethylsilyl ethers [5], and into complex ethers of butyl-or phenylboronic acids [6,7]. Acylation is used most widely.…”

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confidence: 99%

Determination of glycols in glycol-containing oligomers using gas-liquid reaction chromatography

et al. 2016

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A method is proposed for the gas-chromatographic determination of glycols as bis(diethoxyphosphoryl)alkanes formed by the Atherton-Todd reaction with diethyl phosphite. Gas-chromatographic and mass-spectrometric characteristics of the derivatives obtained are studied. Conditions of the phosphorylation reaction are optimized. The method is applied to the determination of the residual amounts of glycols in oligomeric glycol-o-phthalates.

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The Comparison of Derivatization Methods for the Determination of Ethylene Glycol in Lubricant Oil Sample by GC/MS

Cited by 2 publications

References 7 publications

On‐fiber Derivatization for Determination of Ethylene Glycol Concentration in Lubricant oil By SPME‐GC/MS

On‐fiber Derivatization for Determination of Ethylene Glycol Concentration in Lubricant oil By SPME‐GC/MS

Determination of glycols in glycol-containing oligomers using gas-liquid reaction chromatography

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