Abstract:The dislocation relaxation maximum has been investigated at frequencies of 5, 10 and 30 MHz. The three (very high-purity) silver crystals of crystallographic orientation (111), (110) and (100) which are given a resolved shear stress of 20 MPa were found to produce dislocation relaxation maximum at 107 K in all the three samples. The ma.xhnum shifts to 117K when measurement is carried out at 10 MHz and to 127 K at 30 MHz. The results reveal that the maximum is orientation independent. The activation energy and … Show more
“…the Niblett-Wilks peak, was absent). Similar results were observed when studying the dislocation relaxation peak in silver [24] (since both gold and silver have high stacking fault energy). The peak occurs in the temperature ranges of 178-168 K at 5 MHz frequency, 186-182 K at 10 MHz frequency, and 237-232 K at 30 MHz frequency.…”
The ultrasonic attenuation in a polycrystal gold crystal of purity 99.999% has been measured at three different frequencies, 5, 10, and 30 MHz, from 77 to 300 K. Mainly one peak (the dislocation relaxation peak, or Bordoni peak) was observed at 178 - 174, 186 - 185, and 237 - 235 K at 5, 10, and 30 MHz respectively. The highest peak temperature observed was for samples given a low stress (8 MPa) while the lowest was for 130 MPa stress. On further increasing the stress to 259 MPa, the peak temperature increases slightly.
The present work shows that the peak height decreases as the frequency of measurement increases while it increases as the mechanical stress increases. The activation energy and the attempt frequency decrease as the compression deformation to the sample increases.
“…the Niblett-Wilks peak, was absent). Similar results were observed when studying the dislocation relaxation peak in silver [24] (since both gold and silver have high stacking fault energy). The peak occurs in the temperature ranges of 178-168 K at 5 MHz frequency, 186-182 K at 10 MHz frequency, and 237-232 K at 30 MHz frequency.…”
The ultrasonic attenuation in a polycrystal gold crystal of purity 99.999% has been measured at three different frequencies, 5, 10, and 30 MHz, from 77 to 300 K. Mainly one peak (the dislocation relaxation peak, or Bordoni peak) was observed at 178 - 174, 186 - 185, and 237 - 235 K at 5, 10, and 30 MHz respectively. The highest peak temperature observed was for samples given a low stress (8 MPa) while the lowest was for 130 MPa stress. On further increasing the stress to 259 MPa, the peak temperature increases slightly.
The present work shows that the peak height decreases as the frequency of measurement increases while it increases as the mechanical stress increases. The activation energy and the attempt frequency decrease as the compression deformation to the sample increases.
The Bordoni peak in high-purity silver single crystals has been investigated by measuring the attenuation of longitudinal waves of 5, 10 and 30 MHz, using a conventional ultrasonic pulse technique with single quartz transducer. The crystals, of (100), (110) and (111) orientations, were deformed by compression, and the temperature-dependent ultrasonic attenuation was measured after applying resolved shear stresses ranging up to 60 N mm-2. The results lead to the following conclusions: (i) the temperature of the Bordoni peak in silver single crystals is essentially independent of the orientation; (ii) the temperature of the Bordoni peak in silver single crystals decreases as the prior deformation is increased up to resolved shear stress near 28 N mm-2, and then increases for higher prior stresses, (iii) the Bordoni peak height decreases as the frequency increases and (iv) the Bordoni peak height increases with increasing the amount of deformation.
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