The combined third and fourth irradiation in the Advanced Gas Reactor (AGR) program (AGR-3/4) contained tristructural isotropic (TRISO)-coated particle fuel and designed-to-fail (DTF) fuel particles. The DTF particles were only coated with highly anisotropic pyrocarbon (PyC) so they would purposely fail during the AGR-3/4 irradiation and provide a source of fission products for measurement. Frickey performed materialographic preparation of the irradiated and unirradiated fuel compacts. This included designing and fabricating the mounts, grinding, and polishing the mounts at the Hot Fuel Examination Facility at Idaho National Laboratory. Cassie Anderson-Thueson assisted in the mounting, grinding, polishing, and optical microscopy work. John Stanek and Francine Rice assisted in the mount design and provided valuable input to sample preparation and microscopy processes leading to acquisition of the images included in this report. Fuel burnup and fast neutron fluence were calculated by Dr. Jim Sterbentz. Fuel temperatures and temperature variations were calculated by Grant Hawkes.