Water pollution is one of the most important problems in our days, the wastewater discharged by the textile industry exemplifies this problem because high concentrations of colorants and other organic compounds (additives, surfactants, etc.) have been reported from of this sector in aquatic ecosystems. The colorants in water bodies are slowly degraded, generating byproducts of greater toxicity that are easily bioaccumulative, consequently dissolved oxygen is reduced, and biogeochemical cycles are altered, affecting organisms at different trophic levels. The results obtained from the photocatalytic evaluation of Fe 3 O 4 and the Fe 3 O 4 /TiO 2 and Fe 3 O 4 /TiO 2 -βCD complexes indicated that Fe 3 O 4 is the material that degrades in the highest percentage to the orange II azo dye, under a process of exposure to natural sunlight, in addition to showing adequate recoverability and reuse efficiency. Fe 3 O 4 was synthesized by a simple precipitation technique, shows a particle size of 100.617 ± 42.043 nm, a surface charge of -12.133 ± 0.32 mV, a reflectance of 48.218 ± 0.258% at 900 nm wavelength and bandgap energy of 2.95 eV. The experiments related to the reuse of Fe 3 O 4 for 5 cycles indicated that it maintained adequate efficiency, since the degradation percentages remained above 90% for up to three consecutive cycles. However, for the fourth and fifth cycles, the percentages of degradation obtained were lower, these being 86.925 ± 0.407% and 78.119 ± 1.770%, respectively. Thanks to its paramagnetic properties, the easy recovery through the use of a magnet and the degradation percentages obtained, the synthesized Fe 3 O 4 proves to be an alternative for the environmental restoration of contaminated water, this textile dye in areas with optimal solar radiation conditions.