“…It is also obvious from the figure that the Vickers microhardness values are load dependent for all samples; the calculated microhardness value decreases non-linearly as the applied load increased until 1 N, then it tends to attain saturation. This non-linearity has also been observed for Bi-Pb-Sr-Ca-Cu-O samples [26][27][28], for MgB 2 samples [5,6] and it …”
“…It is also obvious from the figure that the Vickers microhardness values are load dependent for all samples; the calculated microhardness value decreases non-linearly as the applied load increased until 1 N, then it tends to attain saturation. This non-linearity has also been observed for Bi-Pb-Sr-Ca-Cu-O samples [26][27][28], for MgB 2 samples [5,6] and it …”
“…The rapid variation of microhardness was observed with increasing applied load from 0.245 to 1.96 N. The reason for this behaviour is due to the contribution of weak grain boundaries and to the process of crack formation along grain boundaries [40]. A similar result was observed for Bi-2223 samples [26,28,29] and is known as indentation size effect (ISE) [41][42][43][44]. The indenter gives geometrically similar indentation; hence, it follows that the measured hardness must be independent of the applied load.…”
Section: Mechanical Measurementssupporting
confidence: 64%
“…Many studies of doping into superconductor oxide ceramics have been made in order to improve their mechanical and superconducting properties [25][26][27][28][29][30]. Engineering applications of high critical temperature (T c ) superconducting ceramics are generally restricted because of their brittleness.…”
“…This non-linear behavior has also been observed in the literature for Bi-Pb-Sr-Ca-Cu-O samples [17,20,28] and is known as indentation size effect (ISE) [29][30][31][32]. To account for this effect, several relationships between the applied load and the resulting indentation size have been suggested [33][34][35][36].…”
In this study we have investigated the influence of iron diffusion and diffusion-annealing time on the mechanical and the superconducting properties of bulk Bi 1.8 Pb 0.35 Sr 1.9 Ca 2.1 Cu 3 O y superconductors by performing X-ray diffraction (XRD), scanning electron microscopy (SEM), Vickers hardness, dc resistivity (q-T) and critical current density (J c ) measurements. The samples are prepared by the conventional solid-state reaction method. Doping of Bi-2223 was carried out by means of iron diffusion during sintering from an evaporated iron film on pellets. Then, the Fe layered superconducting samples were annealed at 830°C for 10, 30 and 60 h. The mechanical properties of the compounds have been investigated by measuring the Vickers hardness (H v ). The mechanical properties of the samples were found to be load dependent. The load independent Vickers hardness (H 0 ), Young's modulus (E), yield strength (Y), and fracture toughness (K IC ) values of the samples are calculated. These all measurements showed that the values of the Vickers hardness, critical current density, and critical transition temperature and lattice parameter c increased with increasing Fe doping and diffusion-annealing time.
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