1995
DOI: 10.1007/bf02547423
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Temperature calibration of differential scanning calorimeters

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Cited by 42 publications
(13 citation statements)
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“…Hysteresis in the transition between crystal structures is not unusual and has been observed in other systems [13,14]. One approach to establishing the absolute limit of this discrepancy between the transition point on cooling and that seen on heating is to observe the transition at progressively slower rates of temperature change and extrapolating the measurements to zero heating and cooling rates [15]. Figure 2 shows stepwise isothermal modulated temperature DSC measurements on silver iodide.…”
Section: Methodsmentioning
confidence: 85%
“…Hysteresis in the transition between crystal structures is not unusual and has been observed in other systems [13,14]. One approach to establishing the absolute limit of this discrepancy between the transition point on cooling and that seen on heating is to observe the transition at progressively slower rates of temperature change and extrapolating the measurements to zero heating and cooling rates [15]. Figure 2 shows stepwise isothermal modulated temperature DSC measurements on silver iodide.…”
Section: Methodsmentioning
confidence: 85%
“…A baseline was subtracted, and the temperatures of phase coexistence onset and completion were determined using the model-free tangent construction method [40,41]. Additional analysis details are found in Supplementary Materials S2.…”
Section: Methodsmentioning
confidence: 99%
“…As they emerge from the bottom of the column, they are detected by a differential refractometer. Since the molecular size in solution (hydrodynamic volume) is related to M w (molecular weight), a picture of the entire M w distribution is obtained quickly and simply [13]. …”
Section: Methodsmentioning
confidence: 99%