Systematic variation of design aspects for a significant increase in thermal fracture resistance of alumina microthrusters

Abstract

Because of thermal stresses occurring upon rapid heating or cooling, microcomponents made from high-temperature co-fired ceramics (HTCC) often fail at temperatures far below what the materials can withstand per se. This work investigates how resistance to thermal fracture in HTCC microcomponents can be increased by improving the component design, aiming at increasing the thermal performance of a microthruster with integrated heaters. The effect of four design parameters: component and cavity geometries (circular or square), heater location (central or peripheral), and addition of embedded platinum layers, on thermal fracture resistance was investigated through a full factorial designed experiment. Components of different designs were manufactured, and their thermal fracture resistance tested by rapid heating until failure. Peripheral heater location and presence of embedded platinum layers were seen to improve resistance to thermal fracture, whereas the shape of the component and the cavity did not significantly affect thermal performance. The most favourable design was then used for a cold gas microthruster that was fabricated and evaluated with respect to thermal fracture resistance. The microthruster survived rapid heating up to 1460 • C and was operated as a cold gas thruster at temperatures up to 772 • C, which is more than twice the maximum temperatures previously reported for alumina microthrusters.

A new method for preventing stress cracking in repairable ceramic packages by changing the sealing ring shape

“…Although the content of Al 2 O 3 in the ceramic substrate is up to 95.0 wt%, a large quantity of micro holes exists in the ceramic, as shown in the supplementary section S2. The ceramic may fracture, even though the tensile stress is lower than the fracture strength of Al 2 O 3 [39,40].…”