Synthesis, Spectroscopic Analysis, and Anti-Bacterial Studies of Pd(II) Complexes of Phosphine and Hydrazone Derivatives
Laith H. K. AL-JİBORİ,
Ahmed SHAKER MARMUS
Abstract:This study reports the synthesis of seven hydrazone derivative complexes by the treatment equivalent molar of the phosphine ligand Ph2P(CH2)nPPh2 {where n= 1 dppm; n=2 dppe; n=3 dppp; n=4
dppb; (CH2)n = (Cp)2Fe} with [Pd(dbeoz)2] afforded complexes of the type [Pd(dbeoz)2(diphos)] and [Pd(dbeoz)2(dppm)]2, whereas the reaction of two moles of Ph3P with [Pd(dbeoz)2] gave a complex [Pd(dbeoz)2(PPh3)2] in good yield. CHN analysis, conductivity measurements, Fourier Transform Infrared (FT-IR), 1H, and 31P-NMR, were… Show more
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