Synthesis of some sym-triazole derivatives

Новиков, С. С.; Brusnikina, V. M.; Rudenko, V. V.

doi:10.1007/bf01031788

Cited by 3 publications

(1 citation statement)

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“…r Jimenez et al, 1989. s The hydroxy-functionalized analog (CAS no. 22250-36-8) has been synthesized and is a solid (Norikov et al, 1969 Sukhanov et al, 2005. v Xue et al, 2004 Kabo et al, 1993. x Kozyro et al, 1990. y Measured value for 402-473 K (Cundall et al, 1978 Majer and Svoboda, 1985. d Measured value for 293-309 K .…”

Section: Enthalpy Of Vaporization and Enthalpy Of Sublimation Estimatesmentioning

confidence: 99%

Property Predictions for Nitrate Salts with Nitroxy-Functionalized Cations

McQuaid¹,

Drake²

2011

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Section: Enthalpy Of Vaporization and Enthalpy Of Sublimation Estimatesmentioning

confidence: 99%

Property Predictions for Nitrate Salts with Nitroxy-Functionalized Cations

McQuaid¹,

Drake²

2011

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A novel type of twisted antiparallel double-chain structure with stacking between the two strands. Structure, synthesis and magnetic properties of [{[Cu₃L₂(dien)(H₂O)₂]·3H₂O}_∞][L = 1H-1,2,4-triazole-3,5-dicarboxylate(3–), dien = 3-Azapentane-1,5-diamine]

Koningsbruggen¹,

Hal²,

Müller³

et al. 1993

J. Chem. Soc., Dalton Trans.

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The synthesis and structure of a completely new type of copper(i1) polymer [{[Cu,L,(dien)-( H20),]-3H20},], where L = 1 H-l,2,4-triazole-3,5-dicarboxylate(3-) and dien = diethylenetriamine (1.4,7-triazaheptane), is reported. The compound crystallizes in the tetragonal space group P42,c. with a = b = 15.845(3), c = 22.743(1) A and Z = 8. Least-squares refinement of 818 reflections with / > 2 0 ( / ) and 174 parameters gave R = 0.0694, R' = 0.0969. The polymer is essentially a double chain, the building blocks of which are trinuclear copper(ii) entities arranged zigzag clockwise and anticlockwise parallel to each other. The copper-copper distances within the trinuclear unit are Cu(1) Cu(2) 5.937(4), Cu(1) Cu(3) 4.014(6) and Cu(2) -.. Cu(3) 5.937(4) A. The two strands of the chain are linked to each other by apical Cu-0 bonds with Cu(2) 9 Cu(2') 3.498(6)A. The magnetic susceptibility data (5.8-284 K) are interpreted on the basis of an exchangeHamiltonian function giving J,[Cu(l)-Cu(3)] = -30.0 cm-l, J2[Cu(2)-Cu(2')] = -1.5 cm-l and g = 2.0. The nature and the strength of the antiferromagnetic exchange are discussed on the basis of the structural features, and compared with previously reported magneto-structural data for related copper(ii) compounds with N1,N2and N1,N4-linked 12.4-triazole ligands.

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Recent approaches to the synthesis of high explosive and energetic materials: A review

Spear¹,

Wilson²

1984

Journal of Energetic Materials

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Synthesis of some sym-triazole derivatives

Cited by 3 publications

References 0 publications

Property Predictions for Nitrate Salts with Nitroxy-Functionalized Cations

Property Predictions for Nitrate Salts with Nitroxy-Functionalized Cations

A novel type of twisted antiparallel double-chain structure with stacking between the two strands. Structure, synthesis and magnetic properties of [{[Cu₃L₂(dien)(H₂O)₂]·3H₂O}_∞][L = 1H-1,2,4-triazole-3,5-dicarboxylate(3–), dien = 3-Azapentane-1,5-diamine]

Recent approaches to the synthesis of high explosive and energetic materials: A review

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Synthesis of some sym-triazole derivatives

Cited by 3 publications

References 0 publications

Property Predictions for Nitrate Salts with Nitroxy-Functionalized Cations

Property Predictions for Nitrate Salts with Nitroxy-Functionalized Cations

A novel type of twisted antiparallel double-chain structure with stacking between the two strands. Structure, synthesis and magnetic properties of [{[Cu3L2(dien)(H2O)2]·3H2O}∞][L = 1H-1,2,4-triazole-3,5-dicarboxylate(3–), dien = 3-Azapentane-1,5-diamine]

Recent approaches to the synthesis of high explosive and energetic materials: A review

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A novel type of twisted antiparallel double-chain structure with stacking between the two strands. Structure, synthesis and magnetic properties of [{[Cu₃L₂(dien)(H₂O)₂]·3H₂O}_∞][L = 1H-1,2,4-triazole-3,5-dicarboxylate(3–), dien = 3-Azapentane-1,5-diamine]