Synthesis of Ni–TiN composites through ultrasonic pulse electrodeposition with excellent corrosion and wear resistance

Xia, Fafeng; Jia, Wanchun; Ma, Chunyang; Wang, Jeremy

doi:10.1016/j.ceramint.2017.09.245

Cited by 52 publications

(12 citation statements)

References 27 publications

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“…The PCE method was used for the deposition of Ni-W/TiN nanocomposites on X52 steel substrates in a modified electrolyte solution [20]. The main components of the X52 steel were listed as follows: 98.49 wt % Fe, 1.05 wt % Mn, 0.22 wt % Cr, 0.20 wt % Si, 0.031 wt % C, and 0.009 wt % P. A pure Ni plate (99.98 wt %) was used as the anode, and the X52 steel (50 mm × 25 mm × 5 mm) was used as the cathode.…”

Section: Experimental Methods 21 Materials Preparationmentioning

confidence: 99%

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Influence of Duty Cycle and Pulse Frequency on Structures and Performances of Electrodeposited Ni-W/TiN Nanocomposites on Oil-Gas X52 Steels

et al. 2021

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This paper describes the pulse current electrodeposition (PCE) mediated preparation of Ni-W/TiN nanocomposites. Pulse current electrodeposition (PCE) was used to make Ni-W/TiN nanocomposites. The nanoindentation, wear, and corrosion of deposited Ni-W/TiN nanocomposites were studied using X-ray diffraction (XRD) and scanning electron microscopy (SEM). The influence of pulse frequency (PF) and duty ratio on the shape, structure, phase structure, wear, and corrosion resistance of Ni-W/TiN nanocomposites was studied. When the duty cycle (DC) was 10%, the results demonstrated that a considerable number of fine grains were present on the deposited Ni-W/TiN nanocomposites, forming smooth, uniform, and fine organization. Increasing DC decreased the content of TiN nanoparticles in Ni-W/TiN nanocomposites. The content of TiN nanoparticles reduced from 11.3 wt % to 7.3 wt % by increasing the DC from 10% to 50%. In contrast, as the PF was increased, the TiN content in Ni-W/TiN nanocomposites increased. When the PF was increased from 50 Hz to 150 Hz, the TiN content increased from 6.4 wt % to 9.6 wt %, respectively. Furthermore, with a PF of 150 Hz and a DC of 10%, the produced Ni-W/TiN nanocomposites had an average hardness of 934.3 HV with ~39.8 µm of an average thickness. The weight loss of the Ni-W/TiN nanocomposites was just 17.2 mg at a PF of 150 Hz, demonstrating the excellent wear resistance potential. Meanwhile, the greatest impedance was found in Ni-W/TiN nanocomposites made with a DC of 10% and a PF of 150 Hz, indicating the best corrosion resistance.

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Section: Experimental Methods 21 Materials Preparationmentioning

confidence: 99%

“…Figure 2 shows the surface morphology and size distribution of TiN particles. The surface morphology of TiN particles was provided by the supplier [20]. TiN powder has a particle size of 30 nm on average.…”

Section: Materials Preparationmentioning

confidence: 99%

Influence of Duty Cycle and Pulse Frequency on Structures and Performances of Electrodeposited Ni-W/TiN Nanocomposites on Oil-Gas X52 Steels

et al. 2021

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“…Composite electroplating is widely practiced in industries to limit the coating failures of the electrodeposition method in adverse environmental conditions subjected to the high potential of hydrogen (pH) and low temperature [ 43 ]. Composite electroplating techniques are best suited for the inclusion of metallic or non-metallic particles in the plated layer that enhance tribological, thermal and mechanical properties [ 44 , 45 ]. Therefore, experimental studies on composite-based electrodeposition or electroplating techniques could enhance the surface properties of coating materials that are of industrial relevance.…”

Section: Introductionmentioning

confidence: 99%

The Effect of Zn and Zn–WO3 Composites Nano-Coatings Deposition on Hardness and Corrosion Resistance in Steel Substrate

Kumar

Chandrashekarappa

Kulkarni³

et al. 2021

Materials

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Pure Zn (Zinc) and its Zn–WO3 (Zinc–Tungsten trioxide) composite coatings were deposited on mild steel specimens by applying the electrodeposition technique. Zn–WO3 composites were prepared for the concentration of 0.5 and 1.0 g/L of particles. The influence of WO3 particles on Zn deposition, the surface morphology of composite, and texture co-efficient were analyzed using a variety of techniques, such as X-ray diffraction (XRD) and scanning electron microscopy (SEM) with Energy Dispersive X-ray analysis (EDX). Higher corrosion resistance and microhardness were observed on the Zn–WO3 composite (concentration of 1.0 g/L). The higher corrosion resistance and microhardness of 1.0 g/L Zn–WO3 nanocomposite coatings effectively protect the steel used for the manufacture of products, parts, or systems from chemical or electrochemical deterioration in industrial and marine ambient environments.

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“…Metal/oksit kompozit malzeme üretmek için çok sayıda yöntem mevcuttur. Bu yöntemler arasında döküm [13], seçici korozyon [14], kimyasal indirgenme [15], elektrokaplama [16]…”

Section: Introductionunclassified

“…Metal/oksit kompozit malzeme üretmek için çok sayıda yöntem mevcuttur. Bu yöntemler arasında döküm [13], seçici korozyon [14], kimyasal indirgenme [15], elektrokaplama [16] ve yüksek enerjili dövme [17] [18]. Elde edilen maksimum doygunluk mıknatıslanma değeri (57 emu/g) literatürde benzer malzemelerden elde edilen değerlerin biraz altındadır [18]- [20].…”

Section: Introductionunclassified

Synthesis of Fe3O4/FeO/CoNi composite material and study of its magnetic properties

KUNDURACI¹

2019

Pamukkale J Eng Sci

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Fe3O4/FeO/CoNikompozit malzemesi iki aşamalı proses kullanılarak üretilmiştir. Birinci aşamada, oksit prekürsörü (öncül malzeme) ıslak sentez esaslı Pechini yöntemi kullanılarak düşük sıcaklıkta üretilmiştir. İkinci aşamada prekürsör malzemesi 500, 600, 700 veya 800 °C'ye hidrojen gazı altında ısıtılarak indirgenmiştir ve metal/oksit kompozit malzemesi elde edilmiştir. Farklı sıcaklıklarda üretilen malzemelerin yapısal, morfolojik ve manyetik özellikleri X-ışını kırınımı, tarama elektron mikroskobu ve titreşen örnek manyetometresi kullanılarak incelenmiştir. 600 °C'den 700 °C'ye geçişte manyetik özelliklerde ani değişiklikler gözlenmiştir. Doygunluk mıknatıslanması iki katına çıkarken, koersif kuvvet yarıya inmiştir. Bu değişiklikler manyetik CoNi fazın amorf bir yapıdan kristal bir yapıya geçişiyle ve Fe3O4 fazın parçacık boyutunun yaklaşık olarak iki katına artmasıyla açıklanmıştır. Fe3O4/FeO/CoNi composite materials were produced using a two-step process. In the first step, oxide precursor was produced at low temperature by wet-synthesis based Pechini method. In the second step, the precursor was heated to 500, 600, 700 or 800 °C under reducing hydrogen gas and metal/oxide composite material was obtained. The structural, morphological and magnetic properties of materials produced at different temperatures were investigated using X-ray diffraction, scanning electron microscope and vibrating sample magnetometer. Sudden changes in magnetic properties were observed during transition from 600 °C to 700 °C. The saturation magnetization doubled while coercive force was halved. These changes were explained with the crystallization of magnetic CoNi phase from an amorphous state and nearly doubling of particle size of Fe3O4 phase.

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Synthesis of Ni–TiN composites through ultrasonic pulse electrodeposition with excellent corrosion and wear resistance

Cited by 52 publications

References 27 publications

Influence of Duty Cycle and Pulse Frequency on Structures and Performances of Electrodeposited Ni-W/TiN Nanocomposites on Oil-Gas X52 Steels

Influence of Duty Cycle and Pulse Frequency on Structures and Performances of Electrodeposited Ni-W/TiN Nanocomposites on Oil-Gas X52 Steels

The Effect of Zn and Zn–WO3 Composites Nano-Coatings Deposition on Hardness and Corrosion Resistance in Steel Substrate

Synthesis of Fe3O4/FeO/CoNi composite material and study of its magnetic properties

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