Synthesis of indole-3-thiocarboxaldehyde

Dolenko, E. V.; Usov, V. A.; Timokhina, L. V.; Usova, T. L.; Protasova, L. E.; Воронков, М. Г.

doi:10.1007/bf00472267

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-Thioformylindole and Its Derivatives2

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“…It was prepared by treatment of the corresponding Vilsmeier salt (9b) with aqueous sodium hydrosulfide. Under these conditions N -[(3-indolyl)methylene]-N ,N -dimethylimmonium perchlorate (9a) is hydrolyzed to 3-formylindole [18].…”

Section: -Thioformylindole and Its Derivativesmentioning

confidence: 99%

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Thiocarbonyl compounds from β-substituted vinylald- and -ketimmonium derivatives

Timokhina¹,

Воронков²

2004

Journal of Sulfur Chemistry

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Section: -Thioformylindole and Its Derivativesmentioning

confidence: 99%

“…Thials 10a, c-e have been synthesized by the action of anhydrous sodium hydrosulfide or hydrogen sulfide on the corresponding methineimmonium salts 9 in DMSO or DMF in the temperature range −20 to 20 • C (scheme 6) [9,18].…”

Section: -Thioformylindole and Its Derivativesmentioning

confidence: 99%