“…These results reveal that the carbonyl group of the amino acid ligand was involved in the complex formation. The coordination through the nitrogen of azomethine and oxygen of ν (C-O) of ligand were further evidenced by the appearance of non-ligand bands around 466-504 cm -1 and 528-556 cm -1 were due to M-N and M-O bonds respectively [20,21]. Table 2.IR spectra of ligand and metal complexes…”
“…These results reveal that the carbonyl group of the amino acid ligand was involved in the complex formation. The coordination through the nitrogen of azomethine and oxygen of ν (C-O) of ligand were further evidenced by the appearance of non-ligand bands around 466-504 cm -1 and 528-556 cm -1 were due to M-N and M-O bonds respectively [20,21]. Table 2.IR spectra of ligand and metal complexes…”
“…22,23 Cyclic voltammetry (CV) studies of the complexes were carried out in 10 mmol/L solutions in DMF containing 0.1 mol/L [NBu 4 ][PF 6 ] as supporting electrolyte. Cyclic voltammograms were performed in a potential range of +1.6 to -2.0 V at sweep rates between 25 and 800 mV/s and were initiated from open circuit potential (E i =0).…”
Section: Electrochemical Measurementsmentioning
confidence: 99%
“…33,34 The magnetic data of the Ni(II) complex agree with a d 8 metal ion in an octahedral configuration. 22,35 …”
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