Synthesis of 5(6)-(1-adamantyl)benzimidazoles

Zurabishvili, D. S.; Lomidze, M. O.; Samsoniya, Sh. A.

doi:10.1007/bf02291642

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-(1-adamantyl)-12-diaminobenzene Dihydrochloride (4)1

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2015

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“…The dihydrochloride 4·2HCl was treated with a 10% solution of NaOH to give the 4-(1-adamantyl)-1,2-diaminobenzene 4 as white crystals with mp 135-137ºC, unstable in air. 1-(4-Acetamido-3-aminophenyl)adamantane (5). A solution of nitroamide 2 (2.62 g, 8 mmol) in absolute ethanol (80 ml) was hydrogenated using molecular hydrogen at 21ºC for 6 h (736 mm Hg) in the presence of Raney nickel.…”

Section: -(1-adamantyl)-12-diaminobenzene Dihydrochloride (4)mentioning

confidence: 99%

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Synthesis and reactions of some 5(6)-(1-adamantyl)benzimidazoles

Zurabishvili

Lomidze

Samsoniya

et al. 2008

Chem Heterocycl Comp

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Section: -(1-adamantyl)-12-diaminobenzene Dihydrochloride (4)mentioning

confidence: 99%

“…We have previously reported [4,5] the synthesis and reactions of 5(6)-(1-adamantyl)benzimidazoles. The synthesized benzimidazoles were assayed for their biocide, antihelmintic, antitumor, and anti HIV activity [6,7] revealing compounds with identified activity.…”

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confidence: 99%