Synthesis Methods and Crystallization 2020
DOI: 10.5772/intechopen.93337
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Synthesis Methods in Solid-State Chemistry

Abstract: The synthesis of single crystal is an area of intense activity in the materials science. The obtaining of the single crystal with sufficient dimension for X-ray diffraction depends on several factors including the chemical composition, crystal structure of the reagents, and physical parameters (temperature and pressure). In this context, this chapter is dedicated to the description of the most common synthesis methods of single crystal in the solid-state chemistry: solid-state method, hydrothermal, and slow ev… Show more

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Cited by 6 publications
(5 citation statements)
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References 39 publications
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“…The major drawbacks are that this process is slower as compared to the other 2D nanosheet preparation methods, produces low yield, and also requires a high temperature range between 500 and 2000 °C. For some materials, heating at this high temperature range can also decompose the final product [106][107][108].…”
Section: Solid-state Methodsmentioning
confidence: 99%
“…The major drawbacks are that this process is slower as compared to the other 2D nanosheet preparation methods, produces low yield, and also requires a high temperature range between 500 and 2000 °C. For some materials, heating at this high temperature range can also decompose the final product [106][107][108].…”
Section: Solid-state Methodsmentioning
confidence: 99%
“…The phenomenon of crystallization often takes place after a phase shift and is accompanied by a heat action. It is completed in two steps: emergence and development, (Smida & Marzouki, 2020). A chemical reaction system without a solvent is known as a dry media reaction, solid-state reaction, or solvent-less reaction, (Viruthagiri et al, 2013).…”
Section: Solid-state Methodsmentioning
confidence: 99%
“…Reaction parameters, structural characteristics of the reagents, surface area of the materials, their reactivity, and the thermodynamic free energy change involved with the process are all variables that influence the efficiency and rate of a solid-state reaction. This technique mainly utilizes complex oxides, carbonates, nitrates, hydroxides, oxalates, alkoxides, and other metal salts to create composites [79].…”
Section: Solid-state Reaction Methodsmentioning
confidence: 99%