Abstract:A synthesis procedure was developed and a new carbacylamidophosphate type ligand N,N'-tetraethyl-N''-trifluoroacetylphosphoroustriamide (CF3C(O)NHP(O)(NC2H5)2, HL) that contains C(O)NP(O) chelating fragment was isolated in the crystalline state. A mononuclear erbium complex [Er(HL)3(NO3)3] and a tetranuclear nickel complex [Ni4L4(OCH3)4(CH3OH)4] were isolated in the crystalline state. The suggestion about the type and coordination mode of the ligand in complexes was made based on IR spectroscopic investigation… Show more
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