“…The Mn0,25Fe2,75O4/NiCo2O4 nanocomposite consisted of two combined phases of Mn0,25Fe2,75O4 and NiCo2O4 which proved the composite process was successful. The results of the refinement of each data are following with previous research on Mn0,25Fe2,75O4 and NiCo2O4 [7,9,25]. Mn0,25Fe2,75O4/NiCo2O4 nanocomposites at the angle 30,14˚; 31,26˚; 35,51˚; 36,84˚; 43,41˚; 45,04˚; 53,53˚; 55,81˚; 57,00˚; 59,57˚; 62,82˚; 65,04˚; 75,62 and 77,18˚.…”