Synthesis, fluorescent properties and aggregation of 2,3-dihydroisoindolenylcalix[4]arenes

Rodik, Roman V.; Malytskyi, Volodymyr; Starova, Viktoriia S.; Yegorova, Tatyana V.; Kysil, Andrii I.; Zaporozhets, Olga A.; Voitenko, Zoia; Kаlchеnkо, Vitaly I.

doi:10.1007/s10847-012-0252-3

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“…Isoindole derivatives are widely used for the development of new drugs [1][2][3][4][5][6][7], as dyes, pigments and fluorophores in materials science [1,[8][9][10][11], as well as markers in analytical chemistry [1]. [12], while condensation of 1-aminoisoindole with phthaloyl chloride [13] or o-chloromethylbenzonitrile and further treatment with sodium ethanolate [14]…”

Section: Introductionmentioning

confidence: 99%

Reaction of 1-aminoisoindole with methyl 4-chloro-3-oxobutanoate

et al. 2018

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Condensation of bifunctional 1-aminoisoindole with bis-electrophilic methyl 4-chloro-3-oxobutanoate undergoes regioselectively to afford 2-(chloromethyl)-2-hydroxy-2,6-dihydropyrimido[2,1-a]isoindol-4(3H)-one. The structure of the reaction product was unambiguously established by HMQC and HMBC heteronuclear correlations. The functionalization of the synthesized compound by reactions with a series of aliphatic amines was carried out.

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