The present study describes the preparation of Poly (N-tert-amylacrylamide-coacrylamide/Maleic acid) OMMT denoted as Poly(NTA-co-AM/MA)OMMT. The first step is the synthesis of Poly(NTA-co-AM/MA)OMMT. The second step is the incorporation of OMMT Nanoclay. The properties of the gel can be modified by the OMMT clay. The amount of MA and Nanoclay places essential role in the adsorption. The adsorption rate of dye stuff is slow at the initial and increases further. Keywords: NTA, Maleic acid(MA), Acrylamide, Organically modified montmorillonite nanoclay(OMMT nanoclay).