2018
DOI: 10.1063/1.5039198
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Synthesis and spectroscopic study of CdS nanoparticles using hydrothermal method

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Cited by 8 publications
(5 citation statements)
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“…The diffraction peaks identified at 2θ = 24.91°, 26.65°, 28.29°, 36.70°, 43.77°, and 62.73° angles correspond to the (100), (002), (101), (102), (110), and (104) planes, respectively, indicating a hexagonal phase structure of the thin films. Among these, the (102) and (110) orientations exhibit higher peak intensities, suggesting a preferred directional growth of particles along these planes due to their lower surface energy, a phenomenon that is in agreement with the existing literature [ 48 , 49 , 50 , 51 , 52 ]. This preferred orientation is attributed to the stacking sequence of close-packed Cd planes, with S atoms occupying tetrahedral interstitial sites, emphasizing the significance of these dominant orientations in the crystal growth process [ 53 ].…”
Section: Resultssupporting
confidence: 91%
“…The diffraction peaks identified at 2θ = 24.91°, 26.65°, 28.29°, 36.70°, 43.77°, and 62.73° angles correspond to the (100), (002), (101), (102), (110), and (104) planes, respectively, indicating a hexagonal phase structure of the thin films. Among these, the (102) and (110) orientations exhibit higher peak intensities, suggesting a preferred directional growth of particles along these planes due to their lower surface energy, a phenomenon that is in agreement with the existing literature [ 48 , 49 , 50 , 51 , 52 ]. This preferred orientation is attributed to the stacking sequence of close-packed Cd planes, with S atoms occupying tetrahedral interstitial sites, emphasizing the significance of these dominant orientations in the crystal growth process [ 53 ].…”
Section: Resultssupporting
confidence: 91%
“…Hydrothermal synthesis presents some benefits: being very pure, with a regulated morphology; having a limited size distribution and comprising single crystals; having a high powder reaction rate; having good dispersion in liquid; and being almost pollution-free. What is more, the prepared powder is not conglomerated but is fine-grained, and it does not need high-tech equipment [67].…”
Section: Hydrothermal Methodsmentioning
confidence: 99%
“…The solution temperature was kept at 60 • C and agitated for 3 s. The prepared combination was then placed in a Teflon-lined sealed stainless-steel autoclave and kept at 170 • C in the oven for 24 h. After slowly cooling down to RT, the final product was rinsed with dH 2 O multiple times, using an electrosonic machine; it was then lifted to dry at 50 to 60 • C overnight. Finally, it is possible to collect the yellow powder [67].…”
Section: Hydrothermal Methodsmentioning
confidence: 99%
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“…The formation of the Bi-2223 phase is particularly sensitive to a wide range of factorsSeveral factors can influence the synthesis of materials, such as sintering temperature, thermal processing duration, synthesis environment, precursor compositions, and the incorporation of different cations and anions through doping or replacement [27,28]. From what we can see, Ni2O3 micro Particles considerably enhanced the formation of Bi-2223 phase [5][6][7][8][9][10], suggesting that they may be somewhat compensating for Cu's slowing effect [21,26].…”
Section: Introductionmentioning
confidence: 99%