2003
DOI: 10.2320/matertrans.44.2678
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Synthesis and Characterization of Nanocrystalline Iron Aluminide Intermetallic Compounds

Abstract: Refining grain size to the nanocrystalline level has been suggested as a way of improving strength while enhancing ductility and toughness. In the present study, nanocrystalline iron aluminide intermetallic compounds were synthesized using mechanical alloying, sintering and high velocity oxy-fuel (HVOF) thermal spraying from the elemental powders. The phase changes occurred during milling, thermal spraying and annealing studied from magnetic and structural points of view. XRD, SEM, DSC and dynamic ultra-microh… Show more

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Cited by 22 publications
(11 citation statements)
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“…The presence of approximately 3 to 5 pct Fe 3 Al in the coating has previously been revealed by a careful analysis of X-ray diffraction (XRD) data. [7] Comparatively, in recent XRD analyses of HVOF-sprayed FeAl coatings, Hu et al [30] and Totemeir et al [18] did not find the presence of the Fe 3 Al phase. The TEM analysis carried out in the present work confirmed the presence of large equiaxed Fe 3 Al grains in the fully melted zones (Figure 3(c)).…”
Section: A the Al Loss And Formation Of The Fe 3 Al Phase And Fine Amentioning
confidence: 96%
“…The presence of approximately 3 to 5 pct Fe 3 Al in the coating has previously been revealed by a careful analysis of X-ray diffraction (XRD) data. [7] Comparatively, in recent XRD analyses of HVOF-sprayed FeAl coatings, Hu et al [30] and Totemeir et al [18] did not find the presence of the Fe 3 Al phase. The TEM analysis carried out in the present work confirmed the presence of large equiaxed Fe 3 Al grains in the fully melted zones (Figure 3(c)).…”
Section: A the Al Loss And Formation Of The Fe 3 Al Phase And Fine Amentioning
confidence: 96%
“…HVOF of nanocrystalline iron aluminide It has been suggested by Hu et al [5] that refining the grain size of the starting powders to the nanocrystalline level led to improve the strength of the coating while enhancing ductility and toughness. In their study, nanocrystalline iron aluminide intermetallic compounds powder synthesized by mechanical alloying were used as feedstock materials for HVOF.…”
Section: Utilization Of Ball-milled Powders As Feedstock Materials Fomentioning
confidence: 99%
“…There is a large scope for research in producing massive parts of ultra-fine grained FeAl alloys. [6] Intermetallic alloys based on FeAl are of interest as possible replacements for various stainless steels and heatresistant Fe-Cr-Ni alloys because they have outstanding oxidation/corrosion resistance at high temperatures. [8] The powder-processed FeAl alloy Fe38Al.…”
Section: Iron Aluminidementioning
confidence: 99%