Synthesis and characterization of iron orthophosphate by solution combustion method

Baykan, Demet; Öztaş, Nurşen Altuntaş

doi:10.1016/j.materresbull.2012.08.069

Cited by 10 publications

(4 citation statements)

References 24 publications

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“…He et al 145 immobilized BiVO 4 onto bentonite to obtain the BiVO 4 /bentonite composite by SCS, which featured a larger surface area and better performance than the initial BiVO 4 , and could be easily recovered. Also, a series of other scheelite type oxides with the ABO 4 structure, FePO 4 , 146 ZnWO 4 , 147 and CeVO 4 148 have also been obtained via SCS using glycine or oxalyldihydrazide as fuels.…”

Section: Scheelite Type Oxides (Abo 4 )mentioning

confidence: 99%

Solution combustion synthesis of metal oxide nanomaterials for energy storage and conversion

et al. 2015

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The design and synthesis of metal oxide nanomaterials is one of the key steps for achieving highly efficient energy conversion and storage on an industrial scale. Solution combustion synthesis (SCS) is a time- and energy-saving method as compared with other routes, especially for the preparation of complex oxides which can be easily adapted for scale-up applications. This review summarizes the synthesis of various metal oxide nanomaterials and their applications for energy conversion and storage, including lithium-ion batteries, supercapacitors, hydrogen and methane production, fuel cells and solar cells. In particular, some novel concepts such as reverse support combustion, self-combustion of ionic liquids, and creation of oxygen vacancies are presented. SCS has some unique advantages such as its capability for in situ doping of oxides and construction of heterojunctions. The well-developed porosity and large specific surface area caused by gas evolution during the combustion process endow the resulting materials with exceptional properties. The relationship between the structural properties of the metal oxides studied and their performance is discussed. Finally, the conclusions and perspectives are briefly presented.

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Section: Scheelite Type Oxides (Abo 4 )mentioning

confidence: 99%

Solution combustion synthesis of metal oxide nanomaterials for energy storage and conversion

et al. 2015

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“…The oxidizer to fuel ratio was calculated based on the oxidizing (O) and fuel (F) valencies of the reactants, as reported earlier [29]. The appropriate amounts of the reactants were mixed under constant stirring, and the temperature was raised to 100 C. The dehydrating combustion mixture was then quickly introduced into a furnace, which was pre-heated to 500 C for 10 min, during which time it decomposed in a smoldering combustion process to yield iron orthophosphate.…”

Section: Solution Combustion Methodsmentioning

confidence: 99%

Synthesis of iron orthophosphate catalysts by solution and solution combustion methods for the hydroxylation of benzene to phenol

Baykan

Öztaş

2015

Materials Research Bulletin

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“…Fe(NO3)3.9H2O has an oxidizing power of -15. Urea (U), glycine (G), hexamethylenetetramine (HMTA), carbohydrazide (CH), citric acid (CA) and starch (S) are reducing fuels with the reducing power of +6, +9, +36, +8, +18 and +24, respectively (18). An appropriate amount of fuel and 1 mmol boric acid were added to the iron solution.…”

Section: Synthesismentioning

confidence: 99%

“…In the last years, solution combustion method, which is time-and energysaving method, have gained great attention (17). This method depends on the exothermic redox reaction between metal nitrate (oxidizer) and an appropriate organic fuel (reducing agent) (18). The fuel type, quantity of fuel and composition are the most important parameters affecting the obtained products.…”

Section: Introductionmentioning

confidence: 99%

Solution Combustion Synthesis of Iron Oxyborate (Fe3BO6)

Özer

İçten

2019

Journal of the Turkish Chemical Society Section A: Chemistry

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In this study, iron oxyborate (Fe3BO6) was synthesized through the solution combustion method as a potential anode material for lithium-ion batteries. Urea, glycine, citric acid, carbohydrazide, hexamethylene tetramine, and starch were used as fuel sources and the effects of the fuels were investigated. The obtained materials were structurally characterized by FT-IR, powder-XRD, solid UV-Vis, TGA and VSM. The pure crystalline Fe3BO6 was synthesized at low temperature and short reaction time using glycine-assisted solution combustion method. It was thermally stable up to 945 °C with a non-uniform morphology and a highly porous structure. The magnetic properties were also studied and Fe3BO6 shows antiferromagnetic behavior. Cite this: Ozer D, Icten O. Solution Combustion Synthesis of Iron Oxyborate (Fe3BO6). JOTCSA. 2019;6(2):95-102.

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Synthesis and characterization of iron orthophosphate by solution combustion method

Cited by 10 publications

References 24 publications

Solution combustion synthesis of metal oxide nanomaterials for energy storage and conversion

Solution combustion synthesis of metal oxide nanomaterials for energy storage and conversion

Synthesis of iron orthophosphate catalysts by solution and solution combustion methods for the hydroxylation of benzene to phenol

Solution Combustion Synthesis of Iron Oxyborate (Fe3BO6)

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