Abstract:The reaction of [C 2 B 10 H 11 CH 2 NH 3 ]Cl (3) with [NH 4 ] 6 [Mo 7 O 24 ][H 2 O] 4 in water instantly afforded a white precipitate: crystallization from acetone-hexane thence gave the hybrid dicarborane octamolybdate salt, [C ][MeCN] 2 (8). Similarly, treatment of an acidified solution of Na 2 WO 4 with [C 2 B 10 H 11 CH 2 NH 3 ]Cl (3) in water also yielded a white precipitate: crystallization from acetone-hexane afforded the salt [C 2 B 10 H 11 CH 2 NH=CHMe 2 ] 4 [W 10 O 32 ][H 2 O] 2 [Me 2 CO] 4 (10), whe… Show more
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