2024
DOI: 10.9734/irjpac/2024/v25i4861
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Syntheses and X-ray Structure of N-(Benzothiazol-2-yl)-3-chlorobenzamide

Salif Sow,
Felix Odame,
Ngoné Diouf
et al.

Abstract: The reaction of 3-chloro-benzoyl chloride and 2-aminobenzothiazole in the presence of potassium thiocyanate yielded a yellowish solid C15H10ClN3OS2 (1). Reaction of 1 with cobalt chloride yield a yellowish solid C14H11ClN2O2S (2) which gives crystal suitable for X-ray analyses. The compounds were characterized by elemental analyses FTIR spectroscopy and melting point measurement. Compound 2 crystallizes in the triclinic space group Pī with the following parameters: a = 7.0299(2) Å b = 7.0466(2) Å c = 14.5490(2… Show more

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