Sequential Column Leaching Test by Microemulsifiers 60 CONCLUSIONS 64 PART II. EFFECTS OF ENVIRONMENTAL CONDITIONS ON SURFACTANT-BASED REMEDIATION FROM HYDROPHOBIC ORGANIC CONTAMINATED SOILS 65 Effects of Environmental Conditions 68 MATERIALS AND METHODS 72 Column Experiments with Varying Environmental Conditions 73 Effect of hydraulic conductivity 73 pH effects 75 vi Counter-ion effects Surfactant concentration effects Surfactant solution temperature effects Sandy soil; clay loam ratio effects Surfactant solution flow rate effects Ratio of surfactant solution volume to soil weight effects RESULTS AND DISCUSSIONS Soil Column Test at Optimal Environmental Conditions CONCLUSIONS PART ill. SURFACTANT RECYCLING BY COUNTER-CURRENT SOLVENT EXTRACTION 101 INTRODUCTION 102 Counter-Current Solvent Extraction 104 MATERIALS AND METHODS 105 RESULTS AND DISCUSSIONS 108 CONCLUSIONS 116 GENERAL DISCUSSION, CONCLUSIONS, AND FUTURE STUDIES 117 APPENDIX A. RESULTS OF SHAKER/CENTRIFUGATION EXPERIMENTS 128 APPENDIX B. RESULTS OF SEQUENTIAL LEACHING TEST BY PUMPING FOR LEACH EFFECTIVENESS 137 APPENDIX C. RESULTS OF SURFACTANT-BASED EXPERIMENTS WITH ENVIRONMENTAL VARIABLES 145 APPENDIX D. RESULTS OF COUNTER-CURRENT SOLVENT EXTRACTION EXPERIMENTS FOR SURFACTANT RECYCLING 159 vii APPENDIX E. MATERIALS AND METHODS FOR SOXHLET EXTRACTION APPENDIX F. DETERMINATION OF RESPONSE FACTOR 165 APPENDIX G. CALCULATION EXAMPLE OF SAMPLE CONCENTRATION