“…1 (s, 3H, CH 3 , enol form), 1.12 (s, 3H, CH 3 , enol form), 2.53 (s, 4H), 3.33 (s, 1H). Lit NMR [65]: (400 MHz, CDCl 3 ): 0.85 (s, 3H, ax.CH ), 1.19 (s, 3H, eq.CH 3 ), 2.38 (dd, 2H, J = 1.4, 14.6Hz), 3.38 (d, 2H, J = 14.6 Hz), 4.75 (t, 1H, J = 1.8 Hz). -1-phenylbutane-1,3-dione (8f) [65].…”