Study On The Effect Of Fuels On Phase Formation And Morphology Of Combustion Derived α-Al2O3 And NiO nanomaterials

Raveendra, R.S.

doi:10.5185/amlett.2016.6202

Cited by 3 publications

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“…The type of fuel used in the solution combustion affects the phase formation and morphology of the resulting nanomaterial [ 22 ]. Several fuels being used include urea, glycine, oxalyldihydrazine, carbohydrazide, EDTA, citric acid, and sucrose [ 23 , 24 ].…”

Section: Introductionmentioning

confidence: 99%

“…Several fuels being used include urea, glycine, oxalyldihydrazine, carbohydrazide, EDTA, citric acid, and sucrose [ 23 , 24 ]. The synthesis of metal oxides using the method with several types of fuel has been examined, such as Fe 3 O 4 using glycine [ 25 ], Bi 2 O 3 using urea, glycine, and citric acid [ 26 ], NiO using urea and glycine [ 22 ], and NiFe 2 O 4 using urea. [ 27 ].…”

Section: Introductionmentioning

confidence: 99%

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The effect of fuel on the physiochemical properties of ZnFe2O4 synthesized by solution combustion method

RIYANTI¹,

PURWANINGRUM²,

YULIASARI³

et al. 2022

Turkish Journal of Chemistry

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The synthesis of ZnFe 2 O 4 nanoparticles was performed using the solution combustion method with three types of fuel, namely urea, glycine, and ethylenediamine tetra-acetic acid (EDTA) with precursors (Zn(NO 3 ) 2 .6H 2 O and Fe(NO 3 ) 3 .9H 2 O. The combustion process was conducted in an open space at 300 °C for ± 1 h, resulting in a brownish-black ZnFe 2 O 4 . Meanwhile, the fuel type used in the process affects the physicochemical properties of ZnFe 2 O 4 . XRD analysis showed that ZnFe 2 O 4 synthesized using urea, glycine, and EDTA had spinel structures with crystal sizes of 10.19, 20.34, and 27.21 nm, respectively. The FTIR spectra of ZnFe 2 O 4 synthesized using the three fuel types had Zn-O and Fe-O stretching vibrations. Furthermore, the morphology of ZnFe 2 O 4 synthesized using urea was more homogeneous than glycine and EDTA. The saturation magnetization of ZnFe 2 O 4 synthesized using EDTA was 54.63 emu/g compared to glycine and urea, 50.93 and 44.73 emu/g, respectively. Finally, the surface area of synthesized ZnFe 2 O 4 using urea, glycine, and EDTA were 116.4, 100.6, and 94.2 m 2 /g, respectively.

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Section: Introductionmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

The effect of fuel on the physiochemical properties of ZnFe2O4 synthesized by solution combustion method

RIYANTI¹,

PURWANINGRUM²,

YULIASARI³

et al. 2022

Turkish Journal of Chemistry

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“…Study of effects on product in regards to specific fuel used in the synthesis of a metal oxide through solution combustion method have previously been carried out such as in the synthesis of TiO2 [23] and NiO [24]. Rasouli et al [23] reported that the synthesis of nanocrystalline TiO2 achieved the largest crystalline size with citric acid as fuel followed by urea and glycine.…”

Section: Introductionmentioning

confidence: 99%

“…The results of analysis of specific surface area with SAA for TiO2 sample obtained from the use of glycine have the largest surface area, followed by urea and citric acid. Furthermore, Raveendra et al [24] reported that from the results of SEM analysis, the morphology of NiO synthesized with urea was spherical and uniformly distributed, whereas the morphology of NiO synthesized with glycine was more porous. The crystal size and surface area of the synthesized products are also influenced by fuel variations.…”

Section: Introductionmentioning

confidence: 99%

Hydrazine and Urea Fueled-Solution Combustion Method for Bi2O3 Synthesis: Characterization of Physicochemical Properties and Photocatalytic Activity

Astuti

Elesta

Widodo

et al. 2019

Bull. Chem. React. Eng. Catal.

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Bismuth oxide synthesis using solution combustion method fuelled by hydrazine and urea has been conducted. This study aims to examine the effect of the applied fuels, urea and hydrazine, on product characteristics and photocatalytic activity in degrading rhodamine B dye. Bismuth oxide synthesis was initiated by dissolving bismuth nitrate pentahydrate (Bi(NO3)3.5H2O) in a nitric acid solvent. Fuel was added and then stirred. The solution formed was heated at 300 ºC for 8 hours. The product obtained was then calcined at 700 ºC for 4 hours. Bismuth oxide synthesized with urea (BO1) and hydrazine (BO2) as fuels both obtained form of yellow powder. The formation of bismuth oxide is indicated by the vibrations of the Bi–O–Bi and Bi–O groups and the crystal structure of a-Bi2O3 in both products. Photocatalytic activity test showed that BO1 has a photocatalyst activity in degrading rhodamine B higher than that of BO2 with constant values of 3.83×10-5 s-1 and 3.43×10-5 s-1, respectively. The high photocatalytic activity can be examined through several factors, such as: band gap values, crystal structure, morphology, and surface area, acquired as a result of the use of different fuels in the synthesis process. Copyright © 2020 BCREC Group. All rights reserved

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Novel nano corrosion inhibitor, integrated zinc titanate nano particles: Synthesis, characterization, thermodynamic and electrochemical studies

Sowmyashree

Somya

Kumar³

et al. 2021

Surfaces and Interfaces

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Study On The Effect Of Fuels On Phase Formation And Morphology Of Combustion Derived α-Al2O3 And NiO nanomaterials

Cited by 3 publications

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The effect of fuel on the physiochemical properties of ZnFe2O4 synthesized by solution combustion method

The effect of fuel on the physiochemical properties of ZnFe2O4 synthesized by solution combustion method

Hydrazine and Urea Fueled-Solution Combustion Method for Bi2O3 Synthesis: Characterization of Physicochemical Properties and Photocatalytic Activity

Novel nano corrosion inhibitor, integrated zinc titanate nano particles: Synthesis, characterization, thermodynamic and electrochemical studies

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