“…5c). 51–53 The appearance of S atom peaks was attributed to the existence of SQX in the structure of 1 after immersion. Simultaneously, the N 1s peaks of complex 1 before and after soaking the SQX were analyzed, as shown in Fig.…”
A d-f heterometallic MOF by use of 2,2'-bipyridine-4,4'-dicarboxylic acid ligand (H2LZ) was obtained by the solvothermal synthesis, namely, [EuZn(LZ)2(HCOO)(H2O)3]n (1). The structure analysis shows that compound 1 is composed of...
“…5c). 51–53 The appearance of S atom peaks was attributed to the existence of SQX in the structure of 1 after immersion. Simultaneously, the N 1s peaks of complex 1 before and after soaking the SQX were analyzed, as shown in Fig.…”
A d-f heterometallic MOF by use of 2,2'-bipyridine-4,4'-dicarboxylic acid ligand (H2LZ) was obtained by the solvothermal synthesis, namely, [EuZn(LZ)2(HCOO)(H2O)3]n (1). The structure analysis shows that compound 1 is composed of...
“…The characteristic peaks at 1594, 1516, and 1451 cm −1 are benzene ring stretching vibration peaks. 27 However, only two peaks, 1516 and 1451 cm −1 , can be seen, indicating that the benzene ring has been destroyed at 650 °C. The stretching and anti-stretching vibrational peaks of –SO 2 – in the sulfonic acid group are 1180 and 1130 cm −1 , respectively.…”
Section: Resultsmentioning
confidence: 97%
“…Thermogravimetry is a necessary tool to study the thermal oxidation of organic waste, to obtain the main degradation temperature intervals of the waste and to provide direction for the study process. 27 The analysis was conducted to comprehend the influence of Mn doping during the oxidation process of cation exchange resins (Fig. 2).…”
Section: Resultsmentioning
confidence: 99%
“…According to the previous research on the decomposition process of cationic resin, these three stages can be briefly divided. 27–30 The first stage is the evaporation of equilibrium water (30–225 °C). The resins have been adequately dried before the experiment.…”
Cationic exchange resins are used in nuclear power circuits to remove the nuclide ions to maintain the safe and efficient operation of nuclear power plants.
“…Our group investigated the destruction process of resins using the ternary eutectic carbonate (Li 2 CO 3 –Na 2 CO 3 –K 2 CO 3 ), and demonstrated that this molten salt system was an effective medium to process resins at low temperatures, thereby reducing the volatilization of radionuclides. 17 Antonetti et al 18 conducted pyrolysis experiments on cation exchange resins (CERs) doped with cobalt and cesium and demonstrated that the presence of Co and Cs on the resin inhibited the transfer of sulfur to the gas phase while accelerating the degradation of volatile carbon compounds. Yang et al 19 investigated the volatilization of Cd, Co, Ce, Cs, Pb, and Sr doped with different contents of resins in binary eutectic carbonate (K 2 CO 3 –Na 2 CO 3 ) at 710 °C.…”
The peroxide and superoxide ions in a carbonate melt prompted the oxidation decomposition of resins in an air atmosphere. Uranium compounds had the reaction paths of UO3 → UO2.92 → U3O8 and UO3 → K2U2O7 → K2UO4.
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