Abstract:Liquid-assisted grinding (LAG) has received wide attention in chemical synthesis field. Here, we reported that LAG provides a smart strategy to build macrocyclic cocrystal (MCC), achieving quick modification. The macrocyclic cocrystal has been assembled by electronegative permethylated pillar[5]arenes (EtP5) and electropositive ligands. We select three ligands with strong electron-deficient groups for cocrystal preparation with EtP5 by LAG and judge whether the grinding products are cocrystals by color change,… Show more
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