STUDY OF [Pd(NH3)4](MoO4)x(CrO4)1–x SOLID SOLUTIONS AND PRODUCTS OF THEIR THERMOLYSIS

The development of an approach for the precision determination of thermal strain tensor elements for single crystals using the example of t-Ag0.8Li0.2InSe2

“…This may indicate the presence of additional systematic errors that were not considered during the routine SC-XRD analysis procedure (possibly due to the lack of the external reference standard) or that there is a sufficiently large error in determining the Ag/Li ratio. As we showed earlier, 14,55 both cases can take place. Taking into account the fact that the upper 2θ limit for data collection during SC-XRD analysis was approximately at 66-73°(MoKα radiation) (see Tables S1 and S2 †), and the angular precision of the goniometer ω-axis is 0.005°, it is possible to estimate the relative error of determining the UCP as ∼1 × 10 −4 .…”