Study of gel grown mixed crystals of Ba x Ca(1−x)(IO3)4

Garud, Siddhartha; Mahajan, Nitu; Saraf, K. B.

doi:10.1007/s12034-009-0029-5

Cited by 5 publications

(2 citation statements)

References 10 publications

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“…Single methods for its growth are not applicable [7,8]. These crystals were also doped with impurities such as Fe 3+ and Cu 2+ .…”

Section: Introductionmentioning

confidence: 99%

Study of XRD, FT-IR and Nonlinear Optical Properties of Doped and Undoped Barium Iodate Crystals Grown in Silica Gel

Shitole¹

2012

IJAPM

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Abstract-Single crystals of barium iodate were grown by simple gel technique by single diffusion method. By varying various parameters, optimum conditions for the growth were established. Crystals having different morphologies and habits were obtained. Prismatic, prismatic pyramidal, dendritic crystals were obtained. Some of them were transparent, some were transluscent, and few others were opaque. The crystals were doped by impurities such as Fe 3+ and Cu 2+ . The formation of the compound was verified by X-ray diffractograms. The results were compared with the standard values given in JCPDS file. It confirms that the grown crystals are barium iodate, monohydrate. Structural analysis was carried out using FT-IR technique. It confirms the iodate group of the grown crystals. Nonlinear optical properties were studied by using powder second harmonic generation method. Effect of doping of Fe 3+ and Cu 2+ on the structure and nonlinear optical properties of bulk crystals was studied. Doping has no effect on the structure. Doping of Cu +2 inhibits nonlinear behavior of the substance, while Fe +3 doping of has less negative effect.

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“…Single methods for its growth are not applicable [7,8]. These crystals were also doped with impurities such as Fe 3+ and Cu 2+ .…”

Section: Introductionmentioning

confidence: 99%

Study of XRD, FT-IR and Nonlinear Optical Properties of Doped and Undoped Barium Iodate Crystals Grown in Silica Gel

Shitole¹

2012

IJAPM

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“…In the present work, single diffusion method was used [1][2][3][4][5][6][7][8][9][10]. In actual procedure, 7 cc, 1N acetic acid was taken in a small beaker, to which SMS solution of density 1.04 gm/cc was added drop by drop with constant stirring by using magnetic stirrer, till the pH value 4.2 was set for the mixture.…”

Section: Methodsmentioning

confidence: 99%

Effect of Gel Parameters on the Growth and Nucleation of Lead Iodate Crystals

Girase¹

2013

IJCI

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Synthesis and Characterization of Calcium Iodate, Monohydrate Crystals Grown in Silica Gel

Shitole¹

2014

Recent Trends in Physics of Material Science and Technology

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Simple gel technique was used to grow single crystals of calcium iodate, monohydrate, by single diffusion method. For the growth of crystals, the optimum conditions were established. Crystals having different morphologies like prismatic and prismatic pyramidal were obtained. Few crystals were opaque, some were translucent and some good quality transparent crystals were obtained. Doping of Cu +2 and Fe +3 was done, to study the effect on structure, thermal and nonlinear optical properties. Cell parameters were obtained from the X-ray diffractograms. Structural analysis was done by using FT-IR spectroscopy. TGA and DTA techniques were used to carry out thermal analysis. Nonlinear optical properties were studied using SHG measurements.

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Study of gel grown mixed crystals of Ba x Ca(1−x)(IO3)4

Cited by 5 publications

References 10 publications

Study of XRD, FT-IR and Nonlinear Optical Properties of Doped and Undoped Barium Iodate Crystals Grown in Silica Gel

Study of XRD, FT-IR and Nonlinear Optical Properties of Doped and Undoped Barium Iodate Crystals Grown in Silica Gel

Effect of Gel Parameters on the Growth and Nucleation of Lead Iodate Crystals

Synthesis and Characterization of Calcium Iodate, Monohydrate Crystals Grown in Silica Gel

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