This paper presents the study results of morphology contact and free surface at amorphous metal foils (Fe7Co71Ni12(SiB)10, Fe70Ni10(SiB)10, Fe60Co30(SiB)10) and their analysis of the elemental composition. Using spectral methods of research was allowed to make a comparative analysis size and anisotropy of distribution topological inhomogeneities. A parallel study of spinning foils by Mossbauer spectroscopy and Vibrating sample magnetometer (VSM) possible to determine the magnetic state of the samples.