“…At room temperature (RT), X-ray diffraction (XRD) patterns were obtained on a Siemens D5000 diffractometer using Cu K emission ¼ 1.5460 Å in the angular range of 10 < 2q < 80 with 10 s for each step of 0.02 around the structure to determine the composition. The FullProf [19][20][21] soware was used to analyze the XRD proles. The morphologies and sizes of the samples were studied directly with a Hitachi SU70 Merlin SEM at an acceleration voltage of 3 kV, equipped with an EDXS energy-dispersive X-ray spectrometer, which was used for the elemental analysis of the different phases.…”
The homogeneity of the 0.8(Ba0.8Sr0.2)TiO3–0.2(Bi0.85Yb0.15)FeO3 ceramic, prepared by a solid-state process, was studied and quantitatively analyzed by scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX).
“…At room temperature (RT), X-ray diffraction (XRD) patterns were obtained on a Siemens D5000 diffractometer using Cu K emission ¼ 1.5460 Å in the angular range of 10 < 2q < 80 with 10 s for each step of 0.02 around the structure to determine the composition. The FullProf [19][20][21] soware was used to analyze the XRD proles. The morphologies and sizes of the samples were studied directly with a Hitachi SU70 Merlin SEM at an acceleration voltage of 3 kV, equipped with an EDXS energy-dispersive X-ray spectrometer, which was used for the elemental analysis of the different phases.…”
The homogeneity of the 0.8(Ba0.8Sr0.2)TiO3–0.2(Bi0.85Yb0.15)FeO3 ceramic, prepared by a solid-state process, was studied and quantitatively analyzed by scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX).
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