Structure and Properties of the Boron Carbide Powder Obtained by the Mechanochemical Synthesis of the Carbon Char and Amorphous Boron Mix

The optimal modes (temperature, time, pressure force) of spark plasma sintering (SPS) and hot pressing of boron carbide obtained by various methods are determined. The initial powders were obtained from soot and amorphous boron by the mechanochemical synthesis method, by the high-temperature synthesis (SHS) method and by the carbon reduction method. The structure and the properties of SPS sintered and hot-pressed boron carbide blanks were determined. The highest value of the relative density was achieved during SPS sintering of blanks from B4C powders obtained by mechanosynthesis and SHS methods. It was found out the optimal conditions for sintering blanks from B4C powder obtained by mechanosynthesis. The density value reaches 99.0 rel.% at 1500 °C/25 MPa and sintering time of 45 min. For powders obtained by the SHS method, the density of sintered blanks is 98.5 rel.%. at 1800 °C/30 MPa with sintering time of 45 min. The highest value of the relative density was achieved during the hot pressing of blanks from B4C powders obtained by mechanosynthesis.

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Production of Nanostructured Boron Carbide Ceramics for Industrial Applications

Eremeeva

Kamali

Лизунов

et al. 2022

KEM

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Enhancing Mechanical Properties of Various Sintered Pellets with Nano-Additives

Nguyên

Konyukhov

Nguyen³

2021

DDF

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The impact of Fe, Co, Ni nano-additives on the density, microhardness and bending strength was investigated for several sintered pellets. Fe, Co, Ni nanopowders (NP) were prepared in the size range 67-94 nm using chemical metallurgy techniques. These powders (0.5 wt. %) were dispersed into three sets of micron powders: Co (+0.5 wt. % Co NP); Fe (+0.5 wt. % Fe NP); Fe+0.5wt. % C (+0.5 wt. % Co and 0.5 wt. % Ni NP). Mixtures were further mixed and processed using a magnetic mill and a turbulent mixer. Sintering was carried out using spark plasma sintering (SPS) as well as pressureless sintering (PS). The densities of sintered pellets were found to increase by 2.5-3% (SPS) and 3-5% (PS) in the presence of nano-additives; corresponding increases in microhardness and bending strength were determined to be 7.9-11.1% and 17.9-38.7%, respectively. These results are discussed in terms enhanced packing due to interparticle sliding and the filling of free spaces with the nanodisperse phase.

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On Question of Metals’ Plasticity

Shinkin

2021

DDF

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Straightforward and reverse descriptions are used to describe the metal’s plasticity zone. For the straightforward descriptions of the hardening zone, the “reference” point is the relative deformation εy corresponding to the yield strength σy. The deviation of the relative deformations in the metal hardening zone is measured relative to εy, and the deviation of the normal stresses is measured relative to σy. For the reverse descriptions of the metal hardening zone, the “reference” point is the relative deformation εu corresponding to the ultimate strength σu. The deviation of the relative deformations in the metal hardening zone is measured relative to εu, and the deviation of the normal stresses is measured relative to σu.

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Structure and Properties of the Boron Carbide Powder Obtained by the Mechanochemical Synthesis of the Carbon Char and Amorphous Boron Mix

Cited by 3 publications

References 10 publications

Production of Nanostructured Boron Carbide Ceramics for Industrial Applications

Production of Nanostructured Boron Carbide Ceramics for Industrial Applications

Enhancing Mechanical Properties of Various Sintered Pellets with Nano-Additives

On Question of Metals’ Plasticity

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