“…The disappearance of the Ti peaks after 2.5 h of milling indicates that Ti began to dissolve in Fe lattice and solid solution of Fe(TiB) formed. The similar results were observed in the studies of Karimi et al They reported that during ball milling of Ni 63 Fe 13 Mo 4 Nb 20 alloy, as milling time increases formation of the Ni (Fe, Nb, Mo) solid solution was achieved due to the complete diffusion of Fe, Nb and Mo into the Ni lattice[32]. After 30 h of milling the all crystalline peaks nearly disappeared and the single broad peak continued to expand up to 70 h milling.…”
In this study, amorphous/nanocrystalline Fe 70 Ti 10 B 20 (at.%) alloys were synthesized by using elemental Fe, Ti and B powders under argon gas atmosphere via mechanical alloying method. The powders were ball milled at 20:1 ball to powder ratio and 500 rpm rotating speed up to 70 h. The phase and morphological properties of the synthesized powders were examined by using X-Ray diffractometer and scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM/EDX). The magnetic properties of powders were determined by vibrating sample magnetometer (VSM) at room temperature in the range of 0-20 kOe. It is determined that after 2.5 h of milling Ti and B are started to dissolve in Fe lattice and Fe(TiB) solid solutions formed. XRD analysis revealed that the amorphous structures were formed after 30 h of milling and the crystallite size and lattice strain were found around 8.2 nm and %1.16, respectively. SEM images indicated that the particles were mostly agglomerated and the particles size distribution was in the range of 10-48 μm. Magnetic measurements revealed that after 70 h of milling, the saturation magnetization (M s) and the coercivity (H c) reached about 94 emu/g and 117 Oe.
“…The disappearance of the Ti peaks after 2.5 h of milling indicates that Ti began to dissolve in Fe lattice and solid solution of Fe(TiB) formed. The similar results were observed in the studies of Karimi et al They reported that during ball milling of Ni 63 Fe 13 Mo 4 Nb 20 alloy, as milling time increases formation of the Ni (Fe, Nb, Mo) solid solution was achieved due to the complete diffusion of Fe, Nb and Mo into the Ni lattice[32]. After 30 h of milling the all crystalline peaks nearly disappeared and the single broad peak continued to expand up to 70 h milling.…”
In this study, amorphous/nanocrystalline Fe 70 Ti 10 B 20 (at.%) alloys were synthesized by using elemental Fe, Ti and B powders under argon gas atmosphere via mechanical alloying method. The powders were ball milled at 20:1 ball to powder ratio and 500 rpm rotating speed up to 70 h. The phase and morphological properties of the synthesized powders were examined by using X-Ray diffractometer and scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM/EDX). The magnetic properties of powders were determined by vibrating sample magnetometer (VSM) at room temperature in the range of 0-20 kOe. It is determined that after 2.5 h of milling Ti and B are started to dissolve in Fe lattice and Fe(TiB) solid solutions formed. XRD analysis revealed that the amorphous structures were formed after 30 h of milling and the crystallite size and lattice strain were found around 8.2 nm and %1.16, respectively. SEM images indicated that the particles were mostly agglomerated and the particles size distribution was in the range of 10-48 μm. Magnetic measurements revealed that after 70 h of milling, the saturation magnetization (M s) and the coercivity (H c) reached about 94 emu/g and 117 Oe.
“…The initial slightly increase of M s at the early stage of milling time can be attributed to the formation of solid solution of BCC-Fe(Co, Ni) and also charge transferring between the ferromagnetic atoms. [22]. It was found that with appropriate atomic ratio of the alloy BCC-Fe (Co, Ni), the magnetic moment is increased, whereas much amount of Co or Ni reduces the magnetic moment [8].…”
“…It strongly depends on the chemical composition of the local environment of atoms and their electronic structure. It involves quantum phenomena, such as exchange, crystal-field interaction, inter-atomic hopping and spin-orbit coupling [34].…”
The magnetic and structural properties of nanostructured (Fe75Al25) 100-xBx alloy prepared by mechanical alloying H. Ibn. Gharsallah (a) , M.Azabou (a) , J. J. Suñol (b) , I. López (c) , N. Llorca-Isern (c) , M. Khitouni * (a) ,
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